trichloroacetimidoyl 3-O-allyl-2,4,6-tri-O-benzyl-α-D-mannopyranoside

Base Information

• Chemical Name: trichloroacetimidoyl 3-O-allyl-2,4,6-tri-O-benzyl-α-D-mannopyranoside
• CAS No.: 1032290-64-4
• Molecular Formula: C₃₂H₃₄Cl₃NO₆
• Molecular Weight: 634.984
• Mol file: 1032290-64-4.mol

Synonyms:trichloroacetimidoyl 3-O-allyl-2,4,6-tri-O-benzyl-α-D-mannopyranoside

Chemical Property of trichloroacetimidoyl 3-O-allyl-2,4,6-tri-O-benzyl-α-D-mannopyranoside

Chemical Property:

Purity/Quality:

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Technology Process of trichloroacetimidoyl 3-O-allyl-2,4,6-tri-O-benzyl-α-D-mannopyranoside

There total 1 articles about trichloroacetimidoyl 3-O-allyl-2,4,6-tri-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

3-O-allyl-2,4,6-tri-O-benzyl-D-mannopyranoside (84553-76-4,84558-12-3,127873-81-8,127873-99-8,127875-23-4,127875-30-3) + trichloroacetonitrile (545-06-2) → trichloroacetimidoyl 3-O-allyl-2,4,6-tri-O-benzyl-α-D-mannopyranoside (1032290-64-4)

Guidance literature:

With sodium hydride; In dichloromethane; at 20 ℃; for 0.666667h;

DOI:10.1021/jo8003953

Reference yield:

trichloroacetimidoyl 3-O-allyl-2,4,6-tri-O-benzyl-α-D-mannopyranoside (1032290-64-4) + (N-phenyl)trifluoroacetimidoyl 2,4,6-tri-O-benzyl-D-mannopyranoside → C65H66F3NO11

Guidance literature:

With 4 A molecular sieve; ytterbium(III) triflate; In 1,4-dioxane; diethyl ether; toluene; at -10 ℃; for 0.5h;

DOI:10.1021/jo8003953

upstream raw materials:

3-O-allyl-2,4,6-tri-O-benzyl-D-mannopyranoside

trichloroacetonitrile