7-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-3,5-dimethyl-heptan-1-ol

Base Information

Chemical Name:7-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-3,5-dimethyl-heptan-1-ol
CAS No.:943226-77-5
Molecular Formula:C₂₂H₄₀O₃Si
Molecular Weight:380.643
Hs Code.:

Synonyms:7-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-3,5-dimethyl-heptan-1-ol

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Chemical Property of 7-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-3,5-dimethyl-heptan-1-ol

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Technology Process of 7-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-3,5-dimethyl-heptan-1-ol

There total 4 articles about 7-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-3,5-dimethyl-heptan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: C₂₈H₅₄O₃Si₂

: 943226-77-5
7-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-3,5-dimethyl-heptan-1-ol

Guidance literature:: With 10-camphorsulfoniuc acid; In methanol; at 0 ℃; for 0.75h;
DOI:10.1021/ol0707970

Reference yield:

: C₁₆H₂₆O₃

: 943226-77-5
7-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-3,5-dimethyl-heptan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / NEt₃ / CH₂Cl₂ / 12 h / 20 °C

2: 57 percent / 10-camphorsulfoniuc acid / methanol / 0.75 h / 0 °C

With triethylamine; In methanol; dichloromethane;
DOI:10.1021/ol0707970

Reference yield:

: C₁₆H₂₄O₂

: 943226-77-5
7-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-3,5-dimethyl-heptan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: BH₃*SMe₂ / tetrahydrofuran / 5.5 h / 20 °C

1.2: 66 percent / aq. H₂O₂; aq. NaHCO₃ / tetrahydrofuran / 0 - 20 °C

2.1: 96 percent / NEt₃ / CH₂Cl₂ / 12 h / 20 °C

3.1: 57 percent / 10-camphorsulfoniuc acid / methanol / 0.75 h / 0 °C

With dimethylsulfide borane complex; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol0707970