Technology Process of C28H30Cl2N4O3
There total 7 articles about C28H30Cl2N4O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C33H38Cl2N4O4;
With
hydrogenchloride;
In
isopropyl alcohol;
at 20 ℃;
for 2h;
With
ammonia;
In
water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium carbonate / N,N-dimethyl-formamide / 60 °C
2: thiophene; hydrogen / 5 % platinum on carbon / tetrahydrofuran
3: PS-carbodiimide; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h / 20 °C
4: hydrogen; triethylamine / palladium 10% on activated carbon / tetrahydrofuran / 50 °C
5: dichloromethane / 2 h / 20 °C
6: hydrogenchloride / isopropyl alcohol / 2 h / 20 °C
With
thiophene; hydrogenchloride; PS-carbodiimide; hydrogen; sodium carbonate; benzotriazol-1-ol; triethylamine;
5 % platinum on carbon; palladium 10% on activated carbon;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: PS-carbodiimide; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h / 20 °C
2: hydrogen; triethylamine / palladium 10% on activated carbon / tetrahydrofuran / 50 °C
3: dichloromethane / 2 h / 20 °C
4: hydrogenchloride / isopropyl alcohol / 2 h / 20 °C
With
hydrogenchloride; PS-carbodiimide; hydrogen; benzotriazol-1-ol; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;