sodium ([2-N-(5-chlorothiazol-2-yl)carboxamido]phenyl-β-D-glucopyranoside)uronate

Base Information

Chemical Name:sodium ([2-N-(5-chlorothiazol-2-yl)carboxamido]phenyl-β-D-glucopyranoside)uronate
CAS No.:1309612-58-5
Molecular Formula:C₁₆H₁₄ClN₂O₈S*Na
Molecular Weight:452.805
Hs Code.:

Synonyms:sodium ([2-N-(5-chlorothiazol-2-yl)carboxamido]phenyl-β-D-glucopyranoside)uronate

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Chemical Property of sodium ([2-N-(5-chlorothiazol-2-yl)carboxamido]phenyl-β-D-glucopyranoside)uronate

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Technology Process of sodium ([2-N-(5-chlorothiazol-2-yl)carboxamido]phenyl-β-D-glucopyranoside)uronate

There total 2 articles about sodium ([2-N-(5-chlorothiazol-2-yl)carboxamido]phenyl-β-D-glucopyranoside)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1309612-57-4
methyl ([2-N-(5-chlorothiazol-2-yl)carboxamido]phenyl-2,3,4-tri-O-acetyl-β-D-glucopyranoside)uronate

: 1309612-58-5
sodium ([2-N-(5-chlorothiazol-2-yl)carboxamido]phenyl-β-D-glucopyranoside)uronate

Guidance literature:: methyl ([2-N-(5-chlorothiazol-2-yl)carboxamido]phenyl-2,3,4-tri-O-acetyl-β-D-glucopyranoside)uronate; With sodium hydroxide; In methanol; at 0 ℃; for 2h;

With acetic acid; In ethanol;
DOI:10.1021/jm200153p

Reference yield:

: 221287-90-7
methyl 1-(2-carboxyphenyl)-2,3,4-tri-O-acetyl-β-D-glucopyranuronate

: 1309612-58-5
sodium ([2-N-(5-chlorothiazol-2-yl)carboxamido]phenyl-β-D-glucopyranoside)uronate

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methyl-morpholine; dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 72 h / 0 °C

2: sodium hydroxide / methanol / 2 h / 0 °C

With 4-methyl-morpholine; dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; dichloromethane;
DOI:10.1021/jm200153p