Technology Process of C64H70N2O8
There total 7 articles about C64H70N2O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine;
In
dichloromethane;
at 0 - 20 ℃;
for 7h;
DOI:10.1016/j.tetlet.2011.08.158
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 2 h / -10 °C / Molecular sieve
2: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 20 °C
3: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C
4: triethylamine / dichloromethane / 0 - 20 °C
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 0 - 20 °C
6: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / dichloromethane / 7 h / 0 - 20 °C
With
2,6-dimethylpyridine; dmap; 2,4,6-trichlorobenzoyl chloride; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2011.08.158
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 20 °C
2: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C
3: triethylamine / dichloromethane / 0 - 20 °C
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 0 - 20 °C
5: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / dichloromethane / 7 h / 0 - 20 °C
With
2,6-dimethylpyridine; dmap; 2,4,6-trichlorobenzoyl chloride; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2011.08.158
