4,4-Dimethyl-3-phenyl-1,3-thiazol-5-spiro-4'-1,3-thiolan-2'-spiro-2''-tricyclo<3.3.1.1^3,7>decan

Base Information

• Chemical Name: 4,4-Dimethyl-3-phenyl-1,3-thiazol-5-spiro-4'-1,3-thiolan-2'-spiro-2''-tricyclo<3.3.1.1^3,7>decan
• CAS No.: 138197-25-8
• Molecular Formula: C₂₂H₂₇NS₃
• Molecular Weight: 401.661

Synonyms:4,4-Dimethyl-3-phenyl-1,3-thiazol-5-spiro-4'-1,3-thiolan-2'-spiro-2''-tricyclo<3.3.1.1^3,7>decan

Chemical Property of 4,4-Dimethyl-3-phenyl-1,3-thiazol-5-spiro-4'-1,3-thiolan-2'-spiro-2''-tricyclo<3.3.1.1^3,7>decan

Chemical Property:

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Technology Process of 4,4-Dimethyl-3-phenyl-1,3-thiazol-5-spiro-4'-1,3-thiolan-2'-spiro-2''-tricyclo<3.3.1.1^3,7>decan

There total 1 articles about 4,4-Dimethyl-3-phenyl-1,3-thiazol-5-spiro-4'-1,3-thiolan-2'-spiro-2''-tricyclo<3.3.1.1^3,7>decan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2',5'-dihydrospiro[adamantane-2,2'-(1,3,4)-thiadiazole] (31934-33-5) + 4,4-dimethyl-2-phenyl-1,3-thiazole-5(4H)-thione (81837-94-7) → 4,4-Dimethyl-3-phenyl-1,3-thiazol-5-spiro-4'-1,3-thiolan-2'-spiro-2''-tricyclo<3.3.1.13,7>decan (138197-25-8)

Guidance literature:

In tetrahydrofuran; at 50 ℃; for 3h;

DOI:10.1002/hlca.19910740703

upstream raw materials:

2',5'-dihydrospiro[adamantane-2,2'-(1,3,4)-thiadiazole]

4,4-dimethyl-2-phenyl-1,3-thiazole-5(4H)-thione

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