3-amino-2,4-dihydroxybenzoic acid

Base Information

• Chemical Name: 3-amino-2,4-dihydroxybenzoic acid
• CAS No.: 860505-23-3
• Molecular Formula: C₇H₇NO₄
• Molecular Weight: 169.137
• Mol file: 860505-23-3.mol

Synonyms:3-amino-2,4-dihydroxybenzoic acid

Chemical Property of 3-amino-2,4-dihydroxybenzoic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-amino-2,4-dihydroxybenzoic acid

There total 6 articles about 3-amino-2,4-dihydroxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-bis-benzyloxy-3-nitrobenzoic acid (1044766-52-0) → 3-amino-2,4-dihydroxybenzoic acid (860505-23-3)

Guidance literature:

With 10% Pd/C; hydrogen; In methanol; at 20 ℃; for 24h; under 760.051 Torr;

DOI:10.1002/anie.200800756

Reference yield:

platensimycin → 3-amino-2,4-dihydroxybenzoic acid (860505-23-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium borohydride / methanol

1.2: sodium phosphate buffer / methanol / pH 7

2.1: aq. HCl / methanol

With hydrogenchloride; sodium tetrahydroborate; In methanol;

DOI:10.1016/j.tetlet.2007.06.009

Reference yield:

C24H30NO7(1-)*Na(1+) → 3-amino-2,4-dihydroxybenzoic acid (860505-23-3) + C17H24O3

Guidance literature:

With hydrogenchloride; In methanol;

DOI:10.1016/j.tetlet.2007.06.009

upstream raw materials:

2,4-bis-benzyloxy-3-nitrobenzoic acid

Downstream raw materials:

(±)-platencin

iso-platencin

(-)-platencin