C₄₀H₅₂N₁₀O₆

Base Information

• Chemical Name: C₄₀H₅₂N₁₀O₆
• CAS No.: 1312610-47-1
• Molecular Formula: C₄₀H₅₂N₁₀O₆
• Molecular Weight: 768.916
• Mol file: 1312610-47-1.mol

Synonyms:C₄₀H₅₂N₁₀O₆

Chemical Property of C₄₀H₅₂N₁₀O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₀H₅₂N₁₀O₆

There total 10 articles about C₄₀H₅₂N₁₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C40H48N10O6S (1312610-46-0) → C40H52N10O6 (1312610-47-1)

Guidance literature:

C₄₀H₄₈N₁₀O₆S; With acetic acid; zinc; In water; at 70 ℃; for 2h;

With sodium hydroxide; In water;

Reference yield:

1,2-diamino-benzene (95-54-5) → C40H52N10O6 (1312610-47-1)

Guidance literature:

Multi-step reaction with 10 steps

1.1: thionyl chloride; triethylamine / dichloromethane / 5 h / Reflux

2.1: bromine; hydrogen bromide / water / 4 h / Reflux

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 12 h / 90 °C / Inert atmosphere

4.1: triethylamine / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 16 h / 120 °C / 15001.5 Torr / Autoclave

5.1: sodium hydroxide; water / tetrahydrofuran / 40 °C

6.1: thionyl chloride / N,N-dimethyl-formamide / 2 h / Reflux

7.1: dichloromethane; diethyl ether / 1 h / -10 - 0 °C

7.2: 1 h / -10 °C

8.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 40 °C

9.1: ammonium acetate / toluene / 100 °C

10.1: zinc; acetic acid / water / 2 h / 70 °C

With thionyl chloride; ammonium acetate; water; hydrogen bromide; bromine; sodium carbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; zinc; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; diethyl ether; dichloromethane; water; toluene; 3.1: Suzuki Coupling;

Reference yield:

4,7-dibromobenzo[c][1,2,5]thiadiazole (15155-41-6) → C40H52N10O6 (1312610-47-1)

Guidance literature:

Multi-step reaction with 8 steps

1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 12 h / 90 °C / Inert atmosphere

2.1: triethylamine / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 16 h / 120 °C / 15001.5 Torr / Autoclave

3.1: sodium hydroxide; water / tetrahydrofuran / 40 °C

4.1: thionyl chloride / N,N-dimethyl-formamide / 2 h / Reflux

5.1: dichloromethane; diethyl ether / 1 h / -10 - 0 °C

5.2: 1 h / -10 °C

6.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 40 °C

7.1: ammonium acetate / toluene / 100 °C

8.1: zinc; acetic acid / water / 2 h / 70 °C

With thionyl chloride; ammonium acetate; water; sodium carbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; zinc; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; diethyl ether; dichloromethane; water; toluene; 1.1: Suzuki Coupling;

upstream raw materials:

1,2-diamino-benzene

4,7-dibromobenzo[c][1,2,5]thiadiazole

methyl 4-(7-bromo-5,6-benzo[c][1,2,5]thiadiazol-4-yl)benzoate

C₁₆H₁₂N₂O₄S

Downstream raw materials:

C₄₁H₅₀N₁₀O₆