1-bromo-4-eicosylbenzene

Base Information

• Chemical Name: 1-bromo-4-eicosylbenzene
• CAS No.: 1293366-53-6
• Molecular Formula: C₂₆H₄₅Br
• Molecular Weight: 437.547
• Mol file: 1293366-53-6.mol

Synonyms:1-bromo-4-eicosylbenzene

Chemical Property of 1-bromo-4-eicosylbenzene

Chemical Property:

Purity/Quality:

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Technology Process of 1-bromo-4-eicosylbenzene

There total 1 articles about 1-bromo-4-eicosylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-4-(2-bromoethyl)benzene (1746-28-7) + n-octadecylmagnesium chloride → 1-bromo-4-eicosylbenzene (1293366-53-6)

Guidance literature:

With buta-1,3-diene; nickel dichloride; In tetrahydrofuran; at -78 - 0 ℃; Inert atmosphere;

DOI:10.1021/ja200498g

Reference yield:

4,9-dihydro-S-indaceno-[1,2-b:5,6-b']-dithiophene-4,9-dione (1209012-30-5) + 1-bromo-4-eicosylbenzene (1293366-53-6) → C68H98O2S2

Guidance literature:

1-bromo-4-eicosylbenzene; With magnesium; In tetrahydrofuran; ethylene dibromide; for 2h; Inert atmosphere; Reflux;

4,9-dihydro-S-indaceno-[1,2-b:5,6-b']-dithiophene-4,9-dione; In tetrahydrofuran; ethylene dibromide; for 12h; Inert atmosphere;

upstream raw materials:

1-bromo-4-(2-bromoethyl)benzene