(2S,3R)-5,7-dimethoxy-2-(3,4,5-trimethoxyphenyl)chroman-3-yl 3,4,5-trimethoxybenzoate

Base Information

Chemical Name:(2S,3R)-5,7-dimethoxy-2-(3,4,5-trimethoxyphenyl)chroman-3-yl 3,4,5-trimethoxybenzoate
CAS No.:121844-31-3
Molecular Formula:C₃₀H₃₄O₁₁
Molecular Weight:570.593
Hs Code.:

Synonyms:(2S,3R)-5,7-dimethoxy-2-(3,4,5-trimethoxyphenyl)chroman-3-yl 3,4,5-trimethoxybenzoate

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Chemical Property of (2S,3R)-5,7-dimethoxy-2-(3,4,5-trimethoxyphenyl)chroman-3-yl 3,4,5-trimethoxybenzoate

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Technology Process of (2S,3R)-5,7-dimethoxy-2-(3,4,5-trimethoxyphenyl)chroman-3-yl 3,4,5-trimethoxybenzoate

There total 1 articles about (2S,3R)-5,7-dimethoxy-2-(3,4,5-trimethoxyphenyl)chroman-3-yl 3,4,5-trimethoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121795-68-4
3,4,5-Trihydroxy-benzoic acid (R)-2-benzylsulfanyl-1-(2,4,6-trihydroxy-benzyl)-2-(3,4,5-trihydroxy-phenyl)-ethyl ester

: 77-78-1
dimethyl sulfate

: 121795-76-4
3,4,5-Trimethoxy-benzoic acid (R)-2-benzylsulfanyl-1-(2,4,6-trimethoxy-benzyl)-2-(3,4,5-trimethoxy-phenyl)-ethyl ester

: 121844-31-3
(2S,3R)-5,7-dimethoxy-2-(3,4,5-trimethoxyphenyl)chroman-3-yl 3,4,5-trimethoxybenzoate

Guidance literature:: With potassium carbonate; In acetone; for 2h; Heating;

Reference yield: 92.0%

: 121844-31-3
(2S,3R)-5,7-dimethoxy-2-(3,4,5-trimethoxyphenyl)chroman-3-yl 3,4,5-trimethoxybenzoate

: 61687-19-2
(2S,3R)-5,7-dimethoxy-2-(3,4,5-trimethoxyphenyl)chroman-3-ol

Guidance literature:: With potassium carbonate; In methanol; 1,2-dimethoxyethane; at 20 ℃; for 10h;
DOI:10.1016/j.ejmech.2021.113795

Reference yield:

: 121844-31-3
(2S,3R)-5,7-dimethoxy-2-(3,4,5-trimethoxyphenyl)chroman-3-yl 3,4,5-trimethoxybenzoate

: (E)-(2S,3R)-5,7-dimethoxy-2-(3,4,5-trimethoxyphenyl)chroman-3-yl 3-(3,4,5-trimethoxyphenyl)acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / methanol; 1,2-dimethoxyethane / 10 h / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere

With dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; 1,2-dimethoxyethane; dichloromethane;
DOI:10.1016/j.ejmech.2021.113795