2-(4-Hydroxy-3,5-dimethylbenzoyl)benzoic acid

Base Information

Chemical Name:2-(4-Hydroxy-3,5-dimethylbenzoyl)benzoic acid
CAS No.:85604-74-6
Molecular Formula:C16H14 O4
Molecular Weight:270.285
Hs Code.:
DSSTox Substance ID:DTXSID20370893
Wikidata:Q82158063
Mol file:85604-74-6.mol

Synonyms:2-(4-hydroxy-3,5-dimethylbenzoyl)benzoic acid;85604-74-6;Benzoic acid,2-(4-hydroxy-3,5-dimethylbenzoyl)-;SCHEMBL5313383;DTXSID20370893;2-(4-Hydroxy-3,5-dimethylbenzoyl)benzoicacid

Suppliers and Price of 2-(4-Hydroxy-3,5-dimethylbenzoyl)benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-CARBOXY-3',5'-DIMETHYL-4'-HYDROXYBENZOPHENONE 95.00%
10G
$ 1226.97

American Custom Chemicals Corporation
2-CARBOXY-3',5'-DIMETHYL-4'-HYDROXYBENZOPHENONE 95.00%
2.5G
$ 791.07

Total 3 raw suppliers

Chemical Property of 2-(4-Hydroxy-3,5-dimethylbenzoyl)benzoic acid

Chemical Property:

PSA：74.60000
LogP:2.93820
XLogP3:2.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:270.08920892
Heavy Atom Count:20
Complexity:367

Purity/Quality:: 2-CARBOXY-3',5'-DIMETHYL-4'-HYDROXYBENZOPHENONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC(=C1O)C)C(=O)C2=CC=CC=C2C(=O)O

Technology Process of 2-(4-Hydroxy-3,5-dimethylbenzoyl)benzoic acid

There total 3 articles about 2-(4-Hydroxy-3,5-dimethylbenzoyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 85-44-9
phthalic anhydride

: 576-26-1,25134-01-4
2.6-dimethylphenol

: 85604-74-6
2-(4-hydroxy-3,5-dimethylbenzoyl)benzoic acid

Guidance literature:: With aluminium trichloride; 1,1,2,2-tetrachloroethane; at 45 - 47 ℃; for 2h;

Reference yield:

: 2-{(4-Hydroxy-3,5-dimethyl-phenyl)-[(E)-4-hydroxy-3,5-dimethyl-phenylimino]-methyl}-benzoic acid

: 85604-74-6
2-(4-hydroxy-3,5-dimethylbenzoyl)benzoic acid

Guidance literature:: With sulfuric acid; for 0.25h; Yield given; Heating;

Reference yield:

: 3689-45-0
3,3-bis(4-hydroxy-3,5-dimethylphenyl)isobenzofuran-1(3H)-one

: 85604-74-6
2-(4-hydroxy-3,5-dimethylbenzoyl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 2.5 N NaOH, 2) H₂NOH, H₂SO₄ / 1) 65 deg C, 15 min, 2) water, heating, 15 min

2: 5 N H₂SO₄ / 0.25 h / Heating

With sodium hydroxide; sulfuric acid; hydroxylamine;