4-methoxyphenyl O-(2,3,4-tri-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-O-(4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-O-(2,3-di-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Base Information

• Chemical Name: 4-methoxyphenyl O-(2,3,4-tri-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-O-(4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-O-(2,3-di-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside
• CAS No.: 144367-42-0
• Molecular Formula: C₉₅H₉₂N₂O₃₃
• Molecular Weight: 1789.77

Synonyms:4-methoxyphenyl O-(2,3,4-tri-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-O-(4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-O-(2,3-di-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Chemical Property of 4-methoxyphenyl O-(2,3,4-tri-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-O-(4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-O-(2,3-di-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Chemical Property:

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Technology Process of 4-methoxyphenyl O-(2,3,4-tri-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-O-(4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-O-(2,3-di-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

There total 2 articles about 4-methoxyphenyl O-(2,3,4-tri-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-O-(4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-O-(2,3-di-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

4-methoxyphenyl O-(6-levulinoyl-2,3,4-tri-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-O-(4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-O-(6-O-levulinoyl-2,3-di-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-4,6-di-O-acetyl-2-deoxy-2-phthalim... → 4-methoxyphenyl O-(2,3,4-tri-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-O-(4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-O-(2,3-di-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside (144367-42-0)

Guidance literature:

With hydrazinium monoacetate; In ethanol; toluene; for 0.75h;

DOI:10.1016/S0008-6215(00)90971-6

Reference yield:

acetic anhydride (108-24-7) + 4-methoxyphenyl O-(6-levulinoyl-2,3,4-tri-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-O-(2-deoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranosyl)-(1->4)-O-(6-O-levulinoyl-2,3-di-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-4,6-di-O-acetyl-2-deoxy-2-pht... (144367-41-9) → 4-methoxyphenyl O-(2,3,4-tri-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-O-(4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-O-(2,3-di-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside (144367-42-0)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1016/S0040-4039(00)61248-0

Reference yield:

4-methoxyphenyl O-(2,3,4-tri-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-O-(4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-O-(2,3-di-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside (144367-42-0) → C95H88N2O33

Guidance literature:

With oxalyl dichloride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; Yield given. Multistep reaction; 1.) CH₂Cl₂, 5 h, 2.) CH₂Cl₂, 10 min;

DOI:10.1016/S0008-6215(00)90971-6

upstream raw materials:

acetic anhydride

4-methoxyphenyl O-(6-levulinoyl-2,3,4-tri-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-O-(2-deoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranosyl)-(1->4)-O-(6-O-levulinoyl-2,3-di-O-p-toluoyl-β-D-glucopyranosyl)-(1->3)-4,6-di-O-acetyl-2-deoxy-2-pht...

Downstream raw materials:

4-methoxyphenyl O-(2,3,4-tri-O-p-toluoyl-β-D-glucopyranosyluronic acid)-(1->3)-O-(4,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-O-(2,3-di-O-p-toluoyl-β-D-glucopyranosyluronic acid)-(1->3)-4,6-di-O-acetyl-2-deoxy-2-phthalimido-β...

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