C₃₆H₄₂N₂O₉

Base Information

• Chemical Name: C₃₆H₄₂N₂O₉
• CAS No.: 1227009-31-5
• Molecular Formula: C₃₆H₄₂N₂O₉
• Molecular Weight: 646.737
• Mol file: 1227009-31-5.mol

Synonyms:C₃₆H₄₂N₂O₉

Chemical Property of C₃₆H₄₂N₂O₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₃₆H₄₂N₂O₉

There total 1 articles about C₃₆H₄₂N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

reserpine (50-55-5) + propargyl bromide (106-96-7) → C36H42N2O9 (1227009-31-5) + reserpine (1227009-32-6)

Guidance literature:

reserpine; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at -20 ℃; for 0.25h;

propargyl bromide; In N,N-dimethyl-formamide; toluene; mineral oil; at -20 ℃; for 1h;

DOI:10.1002/chem.200903264

Reference yield: 75.0%

C36H42N2O9 (1227009-31-5) + (4S,5S)-4,5-bis(azidomethyl)-2,2-dimethyl-1,3-dioxolane (146144-45-8) → C79H96N10O20 (1227009-42-8)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In N,N-dimethyl-formamide; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1002/chem.200903264

Reference yield: 61.0%

C36H42N2O9 (1227009-31-5) → C72H82N4O18 (1227009-37-1)

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; copper(l) chloride; In dichloromethane; at 20 ℃; for 5h;

DOI:10.1002/chem.200903264

upstream raw materials:

reserpine

propargyl bromide

Downstream raw materials:

C₇₂H₈₂N₄O₁₈

C₇₉H₉₆N₁₀O₂₀

Refernces