N-benzylidene-1-(2-(5-hydroxypentyl)-4,4,5,5-tetramethyl-1,3-dioxolan-2-yl)-2-methoxy-2-oxoethanamine oxide

Base Information

Chemical Name:N-benzylidene-1-(2-(5-hydroxypentyl)-4,4,5,5-tetramethyl-1,3-dioxolan-2-yl)-2-methoxy-2-oxoethanamine oxide
CAS No.:1420293-11-3
Molecular Formula:C₂₂H₃₃NO₆
Molecular Weight:407.507
Hs Code.:

Synonyms:N-benzylidene-1-(2-(5-hydroxypentyl)-4,4,5,5-tetramethyl-1,3-dioxolan-2-yl)-2-methoxy-2-oxoethanamine oxide

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Chemical Property of N-benzylidene-1-(2-(5-hydroxypentyl)-4,4,5,5-tetramethyl-1,3-dioxolan-2-yl)-2-methoxy-2-oxoethanamine oxide

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Technology Process of N-benzylidene-1-(2-(5-hydroxypentyl)-4,4,5,5-tetramethyl-1,3-dioxolan-2-yl)-2-methoxy-2-oxoethanamine oxide

There total 3 articles about N-benzylidene-1-(2-(5-hydroxypentyl)-4,4,5,5-tetramethyl-1,3-dioxolan-2-yl)-2-methoxy-2-oxoethanamine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1420292-99-4
5-(4,4,5,5-tetramethyl-1,3-dioxolan-2-yl)pentan-1-ol

: 141565-14-2,77486-09-0,77486-10-3
N-(2-methoxy-2-oxoethylidene)-1-phenylmethanamine N-oxide

: 1420293-11-3
N-benzylidene-1-(2-(5-hydroxypentyl)-4,4,5,5-tetramethyl-1,3-dioxolan-2-yl)-2-methoxy-2-oxoethanamine oxide

Guidance literature:: With tert.-butylhydroperoxide; 1,10-Phenanthroline; Copper(I); benzoate; sodium hydrogencarbonate; In dimethyl sulfoxide; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/asia.201200359

Reference yield:

: 28995-69-9
6,6-dimethoxyhex-1-ene

: 1420293-11-3
N-benzylidene-1-(2-(5-hydroxypentyl)-4,4,5,5-tetramethyl-1,3-dioxolan-2-yl)-2-methoxy-2-oxoethanamine oxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trifluoride diethyl etherate / diethyl ether / 20 h / 20 °C / Inert atmosphere

2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

2.2: NaBO₃ / 20 °C / Inert atmosphere

3.1: tert.-butylhydroperoxide; 1,10-Phenanthroline; Copper(I); benzoate; sodium hydrogencarbonate / dimethyl sulfoxide / 5 h / 20 °C / Inert atmosphere

With tert.-butylhydroperoxide; 1,10-Phenanthroline; boron trifluoride diethyl etherate; Copper(I); benzoate; sodium hydrogencarbonate; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide;
DOI:10.1002/asia.201200359

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1420293-11-3
N-benzylidene-1-(2-(5-hydroxypentyl)-4,4,5,5-tetramethyl-1,3-dioxolan-2-yl)-2-methoxy-2-oxoethanamine oxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trifluoride diethyl etherate / diethyl ether / 20 h / 20 °C / Inert atmosphere

2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

2.2: NaBO₃ / 20 °C / Inert atmosphere

3.1: tert.-butylhydroperoxide; 1,10-Phenanthroline; Copper(I); benzoate; sodium hydrogencarbonate / dimethyl sulfoxide / 5 h / 20 °C / Inert atmosphere

With tert.-butylhydroperoxide; 1,10-Phenanthroline; boron trifluoride diethyl etherate; Copper(I); benzoate; sodium hydrogencarbonate; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide;
DOI:10.1002/asia.201200359