5'(S)-C-(thymin-1-ylmethyl)-5'-O-pixyl-3'-O-(tert-butyldimethylsilyl)thymidine

Base Information

Chemical Name:5'(S)-C-(thymin-1-ylmethyl)-5'-O-pixyl-3'-O-(tert-butyldimethylsilyl)thymidine
CAS No.:945851-83-2
Molecular Formula:C₄₁H₄₆N₄O₈Si
Molecular Weight:750.924
Hs Code.:

Synonyms:5'(S)-C-(thymin-1-ylmethyl)-5'-O-pixyl-3'-O-(tert-butyldimethylsilyl)thymidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'(S)-C-(thymin-1-ylmethyl)-5'-O-pixyl-3'-O-(tert-butyldimethylsilyl)thymidine

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Technology Process of 5'(S)-C-(thymin-1-ylmethyl)-5'-O-pixyl-3'-O-(tert-butyldimethylsilyl)thymidine

There total 3 articles about 5'(S)-C-(thymin-1-ylmethyl)-5'-O-pixyl-3'-O-(tert-butyldimethylsilyl)thymidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 945851-69-4
5'(S)-C-(thymin-1-ylmethyl)-3'-O-(tert-butyldimethylsilyl)thymidine

: 42506-03-6
pixyl chloride

: 945851-83-2
5'(S)-C-(thymin-1-ylmethyl)-5'-O-pixyl-3'-O-(tert-butyldimethylsilyl)thymidine

Guidance literature:: In pyridine; for 12h;
DOI:10.1039/b700852j

Reference yield:

: C₁₇H₂₈O₅N₂Si

: 945851-83-2
5'(S)-C-(thymin-1-ylmethyl)-5'-O-pixyl-3'-O-(tert-butyldimethylsilyl)thymidine

Guidance literature:: Multi-step reaction with 2 steps

1: 0.60 g / potassium carbonate / dimethylformamide / 13 h / 20 - 85 °C

2: 79 percent / pyridine / 12 h

With potassium carbonate; In pyridine; N,N-dimethyl-formamide;
DOI:10.1039/b700852j

Reference yield:

: 142325-10-8
5′-deoxy-5′-C-methenyl-3′-O-(tert-butyldimethylsilyl)thymidine

: 945851-83-2
5'(S)-C-(thymin-1-ylmethyl)-5'-O-pixyl-3'-O-(tert-butyldimethylsilyl)thymidine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.62 g / mCPBA / CH₂Cl₂ / 24 h

2: 0.60 g / potassium carbonate / dimethylformamide / 13 h / 20 - 85 °C

3: 79 percent / pyridine / 12 h

With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In pyridine; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b700852j