(1R,2S,5R)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexyl-(2,3-dibromo)propionate

Base Information

Chemical Name:(1R,2S,5R)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexyl-(2,3-dibromo)propionate
CAS No.:635678-43-2
Molecular Formula:C₁₉H₂₆Br₂O₂
Molecular Weight:446.222
Hs Code.:

Synonyms:(1R,2S,5R)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexyl-(2,3-dibromo)propionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,5R)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexyl-(2,3-dibromo)propionate

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Technology Process of (1R,2S,5R)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexyl-(2,3-dibromo)propionate

There total 2 articles about (1R,2S,5R)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexyl-(2,3-dibromo)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 72526-00-2
(-)-8-phenylmenthyl acrylate

: 635678-43-2
(1R,2S,5R)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexyl-(2,3-dibromo)propionate

Guidance literature:: With bromine; In dichloromethane; at 50 ℃; for 0.5h;
DOI:10.1021/jo0352326

Reference yield:

: 65253-04-5
(-)-8-phenylmenthol

: 635678-43-2
(1R,2S,5R)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexyl-(2,3-dibromo)propionate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N; DMAP / CH₂Cl₂ / 0 °C

2: 95 percent / Br₂ / CH₂Cl₂ / 0.5 h / 50 °C

With dmap; bromine; triethylamine; In dichloromethane;
DOI:10.1021/jo0352326

Reference yield:

: 635678-43-2
(1R,2S,5R)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexyl-(2,3-dibromo)propionate

: 600734-37-0
(1R,2S,5R)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexyl 2H-azirine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NaN₃ / dimethylformamide / 0.33 h / 85 °C

2: 100 percent / CH₂Cl₂ / 0.33 h / 150 °C

With sodium azide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0352326