N-<(benzyloxy)carbonyl>-2-(3,4-dimethoxyphenyl)-4-oxo-1,2,3,4-tetrahydropyridine

Base Information

Chemical Name:N-<(benzyloxy)carbonyl>-2-(3,4-dimethoxyphenyl)-4-oxo-1,2,3,4-tetrahydropyridine
CAS No.:116725-72-5
Molecular Formula:C₂₁H₂₁NO₅
Molecular Weight:367.401
Hs Code.:

Synonyms:N-<(benzyloxy)carbonyl>-2-(3,4-dimethoxyphenyl)-4-oxo-1,2,3,4-tetrahydropyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<(benzyloxy)carbonyl>-2-(3,4-dimethoxyphenyl)-4-oxo-1,2,3,4-tetrahydropyridine

Chemical Property:

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Technology Process of N-<(benzyloxy)carbonyl>-2-(3,4-dimethoxyphenyl)-4-oxo-1,2,3,4-tetrahydropyridine

There total 1 articles about N-<(benzyloxy)carbonyl>-2-(3,4-dimethoxyphenyl)-4-oxo-1,2,3,4-tetrahydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 620-08-6,1232006-56-2
4-methoxypyridine

: 2859-78-1
4-Bromoveratrole

: 501-53-1,94274-21-2
benzyl chloroformate

: 116725-72-5
N-<(benzyloxy)carbonyl>-2-(3,4-dimethoxyphenyl)-4-oxo-1,2,3,4-tetrahydropyridine

Guidance literature:: With magnesium; ethylene dibromide; Yield given. Multistep reaction; 1.) THF, r.t., 12 h, 2.) THF, -23 deg C, 4 h;
DOI:10.1021/ja00230a026

Reference yield:

: 116725-72-5
N-<(benzyloxy)carbonyl>-2-(3,4-dimethoxyphenyl)-4-oxo-1,2,3,4-tetrahydropyridine

: 89771-49-3
(±)-lasubine II

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg, 2.) CuBr*S(CH₃)2, boron trifluoride etherate / 1.) diethyl ether, 0 deg C, 1 h, 2.) THF, -78 deg C, 4 h

2: 75 percent / hydrogen, lithium carbonate / 5 percent Pd/C / ethyl acetate / 12 h / 2068.6 Torr

3: 1.) LS-selectride, 2.) 1 N NaOH / 1.) THF, -78 deg C, 30 min, 2.) ethanol, reflux, 1 h

With sodium hydroxide; copper(I) bromide dimethylsulfide complex; boron trifluoride diethyl etherate; hydrogen; lithium carbonate; magnesium; lithium tri-sec-butyl(hydrido)borate; palladium on activated charcoal; In ethyl acetate;
DOI:10.1021/ja00230a026

Reference yield:

: 116725-72-5
N-<(benzyloxy)carbonyl>-2-(3,4-dimethoxyphenyl)-4-oxo-1,2,3,4-tetrahydropyridine

: 89690-20-0,71593-15-2,89690-19-7,112840-40-1,144409-60-9
(4R*,9aR*)-4-(3,4-dimethoxyphenyl)octahydro-2H-quinolizin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg, 2.) CuBr*S(CH₃)2, boron trifluoride etherate / 1.) diethyl ether, 0 deg C, 1 h, 2.) THF, -78 deg C, 4 h

2: 75 percent / hydrogen, lithium carbonate / 5 percent Pd/C / ethyl acetate / 12 h / 2068.6 Torr

With copper(I) bromide dimethylsulfide complex; boron trifluoride diethyl etherate; hydrogen; lithium carbonate; magnesium; palladium on activated charcoal; In ethyl acetate;
DOI:10.1021/ja00230a026