C₂₈H₁₄F₆S₄

Base Information

Chemical Name:C₂₈H₁₄F₆S₄
CAS No.:1422279-59-1
Molecular Formula:C₂₈H₁₄F₆S₄
Molecular Weight:592.674
Hs Code.:

C<sub>28</sub>H<sub>14</sub>F<sub>6</sub>S<sub>4</sub>

Synonyms:C₂₈H₁₄F₆S₄

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Chemical Property of C₂₈H₁₄F₆S₄

Chemical Property:

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Technology Process of C₂₈H₁₄F₆S₄

There total 7 articles about C₂₈H₁₄F₆S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1380426-05-0
2,5-bis(5-bromothiophen-2-yl)thieno[3,2-b]thiophene

: 128796-39-4
4-trifluoromethylphenylboronic acid

: 1422279-59-1
C₂₈H₁₄F₆S₄

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In toluene; for 24h; Schlenk technique; Inert atmosphere; Reflux;
DOI:10.3390/molecules171012163

Reference yield:

: 930-96-1
3-bromo-2-thiophenecarboxaldehyde

: 1422279-59-1
C₂₈H₁₄F₆S₄

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate / N,N-dimethyl-formamide

2: sodium hydroxide

3: copper; quinoline

4: N-Bromosuccinimide / N,N-dimethyl-formamide

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 90 °C / Schlenk technique; Inert atmosphere

6: N-Bromosuccinimide / N,N-dimethyl-formamide / 3.33 h / 0 - 20 °C / Schlenk technique; Inert atmosphere

7: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene / 24 h / Schlenk technique; Inert atmosphere; Reflux

With quinoline; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper; sodium carbonate; potassium carbonate; sodium hydroxide; In N,N-dimethyl-formamide; toluene; 7: |Suzuki Coupling;
DOI:10.3390/molecules171012163

Reference yield:

: 1723-27-9
thieno[3,2-b]thiophene-2-carboxylic acid

: 1422279-59-1
C₂₈H₁₄F₆S₄

Guidance literature:: Multi-step reaction with 5 steps

1: copper; quinoline

2: N-Bromosuccinimide / N,N-dimethyl-formamide

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 90 °C / Schlenk technique; Inert atmosphere

4: N-Bromosuccinimide / N,N-dimethyl-formamide / 3.33 h / 0 - 20 °C / Schlenk technique; Inert atmosphere

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene / 24 h / Schlenk technique; Inert atmosphere; Reflux

With quinoline; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper; sodium carbonate; In N,N-dimethyl-formamide; toluene; 5: |Suzuki Coupling;
DOI:10.3390/molecules171012163