Technology Process of C22H24O4
There total 6 articles about C22H24O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sulfur; morpholine / 12 h / 130 °C
1.2: 12 h / Reflux
2.1: boron trifluoride diethyl etherate / 0.17 h / 100 °C
2.2: 0.33 h / 55 °C
2.3: 3 h / 80 °C
3.1: acetic acid; hydrogen; 5%-palladium/activated carbon / ethanol; water / 12 h / 20 °C
4.1: acetic acid; phenylboronic acid / toluene / 12 h / Reflux; Inert atmosphere
With
morpholine; 5%-palladium/activated carbon; boron trifluoride diethyl etherate; hydrogen; sulfur; acetic acid; phenylboronic acid;
In
ethanol; water; toluene;
DOI:10.1080/00397911.2013.821616
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydroxide / water / 3 h / 0 - 70 °C
2.1: aluminum (III) chloride / dichloromethane / 1 h / 0 - 20 °C
3.1: sulfur; morpholine / 12 h / 130 °C
3.2: 12 h / Reflux
4.1: boron trifluoride diethyl etherate / 0.17 h / 100 °C
4.2: 0.33 h / 55 °C
4.3: 3 h / 80 °C
5.1: acetic acid; hydrogen; platinum on carbon / 12 h / 100 °C
6.1: acetic acid; phenylboronic acid / toluene / 12 h / Reflux; Inert atmosphere
With
morpholine; aluminum (III) chloride; platinum on carbon; boron trifluoride diethyl etherate; hydrogen; sulfur; acetic acid; sodium hydroxide; phenylboronic acid;
In
dichloromethane; water; toluene;
DOI:10.1080/00397911.2013.821616
