N²-(4-isobutyryloxyphenyl)-O⁶-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

Base Information

• Chemical Name: N²-(4-isobutyryloxyphenyl)-O⁶-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine
• CAS No.: 1140395-28-3
• Molecular Formula: C₃₉H₅₇N₅O₆Si₂
• Molecular Weight: 748.082

Synonyms:N²-(4-isobutyryloxyphenyl)-O⁶-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

Chemical Property of N²-(4-isobutyryloxyphenyl)-O⁶-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

Chemical Property:

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Technology Process of N²-(4-isobutyryloxyphenyl)-O⁶-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

There total 1 articles about N²-(4-isobutyryloxyphenyl)-O⁶-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-isobutyryloxybromobenzene (104316-23-6) + O6-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine (236427-57-9) → N2-(4-isobutyryloxyphenyl)-O6-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine (1140395-28-3)

Guidance literature:

With caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In toluene; at 80 ℃; for 6h;

DOI:10.1080/15257770802258034

Reference yield: 88.0%

N2-(4-isobutyryloxyphenyl)-O6-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine (1140395-28-3) → N2-(4-isobutyryloxyphenyl)-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine (1140395-30-7)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 16h; under 2585.81 Torr;

DOI:10.1080/15257770802258034

upstream raw materials:

4-isobutyryloxybromobenzene

O⁶-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

Downstream raw materials:

N²-(4-isobutyryloxyphenyl)-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

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