Technology Process of C50H49N13O10S7
There total 11 articles about C50H49N13O10S7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
trifluoromethane sulfonyl chloride; C49H47N13O8S6;
With
pyridine;
for 0.5h;
With
sodium hydrogencarbonate;
In
water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 14 h / 80 °C
2: pyridine; dmap / dichloromethane / 3 h
3: dichloromethane / 0.5 h
4: pyridine; triethylamine / dichloromethane / 0.5 h
With
pyridine; dmap; triethylamine;
In
dichloromethane;
1: Curtius rearrangement;
DOI:10.1021/jm101602q
- Guidance literature:
-
Multi-step reaction with 8 steps
1: formic acid
2: water; sodium hydroxide / tetrahydrofuran / 1.5 h / 60 °C
3: triethylamine / acetone / Sonication
4: sodium azide / acetone / 1.33 h / 60 °C
5: 14 h / 80 °C
6: pyridine; dmap / dichloromethane / 3 h
7: dichloromethane / 0.5 h
8: pyridine; triethylamine / dichloromethane / 0.5 h
With
pyridine; dmap; formic acid; sodium azide; water; triethylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; acetone;
5: Curtius rearrangement;
DOI:10.1021/jm101602q