2-{6-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]quinolin-2-yl}aniline

Base Information

Chemical Name:2-{6-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]quinolin-2-yl}aniline
CAS No.:194347-19-8
Molecular Formula:C₂₆H₂₅N₅
Molecular Weight:407.518
Hs Code.:

Synonyms:2-{6-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]quinolin-2-yl}aniline

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Chemical Property of 2-{6-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]quinolin-2-yl}aniline

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Technology Process of 2-{6-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]quinolin-2-yl}aniline

There total 11 articles about 2-{6-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]quinolin-2-yl}aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-chloro-6-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]-2-(nitrophenyl)quinoline

: 194347-19-8
2-{6-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]quinolin-2-yl}aniline

Guidance literature:: With potassium hydroxide; palladium-carbon catalyst; In methanol; chloroform; water;

Reference yield:

: 6-(2-ethyl-5,7-dimethyl-imidazo[4,5-b]pyridin-3-ylmethyl)-2-(2-nitro-phenyl)-quinoline

: 194347-19-8
2-{6-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]quinolin-2-yl}aniline

Guidance literature:: With hydrogen; palladium on activated charcoal;
DOI:10.1016/S0022-1139(01)00383-9

Reference yield:

: 608-05-9
5-methyl-indole-2,3-dione

: 194347-19-8
2-{6-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]quinolin-2-yl}aniline

Guidance literature:: Multi-step reaction with 8 steps

1: NaOH

2: quinoline; H₂SO₄

3: SOCl₂

4: NBS

5: NaH

6: Alkaline hydrolysis

7: (PhO)2P(O)N₃; Et₃N

8: Alkaline hydrolysis

With quinoline; sodium hydroxide; N-Bromosuccinimide; thionyl chloride; sulfuric acid; diphenyl phosphoryl azide; sodium hydride; triethylamine; 7: Curtius rearrangement;
DOI:10.1016/S0022-1139(01)00383-9