methyl 5-salicylate

Base Information

Chemical Name:methyl 5-salicylate
CAS No.:152502-18-6
Molecular Formula:C₁₃H₁₆N₂O₆
Molecular Weight:296.28
Hs Code.:

methyl 5-<N-(methyl L-aspartyl ester)amino>salicylate

Synonyms:methyl 5-salicylate

Suppliers and Price of methyl 5-salicylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 5-salicylate

Chemical Property:

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Technology Process of methyl 5-salicylate

There total 3 articles about methyl 5-salicylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 152502-16-4
methyl 5-amino>salicylate

: 152502-18-6
methyl 5-salicylate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 6h; under 2585.7 Torr;
DOI:10.1021/jm00078a009

Reference yield:

: 3160-47-2
N-(benzyloxycarbonyl)-L-aspartic acid 4-methyl ester

: 152502-18-6
methyl 5-salicylate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / DCC, imidazole / ethyl acetate

2: 91 percent / H₂ / 5percent Pd/C / methanol / 6 h / 2585.7 Torr

With 1H-imidazole; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1021/jm00078a009

Reference yield:

: 42753-75-3
methyl 5-amino-2-hydroxybenzoate

: 152502-18-6
methyl 5-salicylate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / DCC, imidazole / ethyl acetate

2: 91 percent / H₂ / 5percent Pd/C / methanol / 6 h / 2585.7 Torr

With 1H-imidazole; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1021/jm00078a009