2-benzenesulfonyl-N-butyl-N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-acetamide

Base Information

• Chemical Name: 2-benzenesulfonyl-N-butyl-N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-acetamide
• CAS No.: 667458-55-1
• Molecular Formula: C₂₀H₃₅NO₄SSi
• Molecular Weight: 413.654

Synonyms:2-benzenesulfonyl-N-butyl-N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-acetamide

Chemical Property of 2-benzenesulfonyl-N-butyl-N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-acetamide

Chemical Property:

Purity/Quality:

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Technology Process of 2-benzenesulfonyl-N-butyl-N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-acetamide

There total 2 articles about 2-benzenesulfonyl-N-butyl-N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

butyl-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-amine → 2-benzenesulfonyl-N-butyl-N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-acetamide (667458-55-1)

Guidance literature:

Multi-step reaction with 2 steps

1: TEA / CH₂Cl₂ / 1 h / 20 °C

2: dimethylformamide / 1 h / 20 °C

With TEA; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ol016647l

Reference yield:

sodium benzenesulfonate (873-55-2) + 2-bromo-N-butyl-N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-acetamide → 2-benzenesulfonyl-N-butyl-N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-acetamide (667458-55-1)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 1h;

DOI:10.1021/ol016647l

Reference yield:

2-benzenesulfonyl-N-butyl-N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-acetamide (667458-55-1) → 2-benzenesulfonyl-N-butyl-N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-2-diazo-acetamide (380370-63-8)

Guidance literature:

With 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 0.5h;

DOI:10.1021/ol016647l

upstream raw materials:

sodium benzenesulfonate

Downstream raw materials:

2-benzenesulfonyl-N-butyl-N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-2-diazo-acetamide

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