2-amino-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide hydrochloride

Base Information

Chemical Name:2-amino-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide hydrochloride
CAS No.:82095-13-4
Molecular Formula:C₂₂H₁₇Cl₃N₂O₂*ClH
Molecular Weight:484.209
Hs Code.:

Synonyms:2-amino-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide hydrochloride

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Chemical Property of 2-amino-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide hydrochloride

Chemical Property:

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Technology Process of 2-amino-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide hydrochloride

There total 10 articles about 2-amino-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 82082-42-6
2-azido-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide

: 82095-13-4
2-amino-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; platinum(IV) oxide; In tetrahydrofuran; ethanol; for 4h; under 760 Torr; Ambient temperature;
DOI:10.1021/jm00351a009

Reference yield:

: 6628-86-0
5-chloro-2-nitrobenzaldehyde

: 82095-13-4
2-amino-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide hydrochloride

Guidance literature:: Multi-step reaction with 9 steps

1: 1.) n-BuLi / 1.) THF, -78 deg C, 20 min, 2.) THF, -78 deg C, 1 h

2: Jones reagent, acetic acid / diethyl ether / 12 h / Ambient temperature

3: 62 percent / H₂ / Raney nickel / ethanol / 8 h / 760 Torr

4: 84 percent / pyridine / diethyl ether; CH₂Cl₂ / 1 h / Ambient temperature

5: 1.) n-BuLi / 1.) hexane, DMSO, 2.) hexane, DMSO, RT, 1 h

6: 70 percent / NaOH / aq. ethanol / 72 h / Heating

7: 100 percent / pyridine / diethyl ether / 0.33 h / Ambient temperature

8: 95 percent / NaN₃ / dimethylsulfoxide / 12 h / Ambient temperature

9: 93 percent / H₂, 6percent methanolic HCl / PtO₂ / tetrahydrofuran; ethanol / 4 h / 760 Torr / Ambient temperature

With pyridine; hydrogenchloride; sodium hydroxide; n-butyllithium; sodium azide; jones reagent; hydrogen; acetic acid; platinum(IV) oxide; nickel; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jm00351a009

Reference yield:

: 82082-26-6
(2,6-dichlorophenyl)(2-amino-5-chlorophenyl)methanone

: 82095-13-4
2-amino-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: 84 percent / pyridine / diethyl ether; CH₂Cl₂ / 1 h / Ambient temperature

2: 1.) n-BuLi / 1.) hexane, DMSO, 2.) hexane, DMSO, RT, 1 h

3: 70 percent / NaOH / aq. ethanol / 72 h / Heating

4: 100 percent / pyridine / diethyl ether / 0.33 h / Ambient temperature

5: 95 percent / NaN₃ / dimethylsulfoxide / 12 h / Ambient temperature

6: 93 percent / H₂, 6percent methanolic HCl / PtO₂ / tetrahydrofuran; ethanol / 4 h / 760 Torr / Ambient temperature

With pyridine; hydrogenchloride; sodium hydroxide; n-butyllithium; sodium azide; hydrogen; platinum(IV) oxide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jm00351a009