Decanedioic acid (4-amino-benzyl)-methyl-amide dimethylamide

Base Information

Chemical Name:Decanedioic acid (4-amino-benzyl)-methyl-amide dimethylamide
CAS No.:74268-85-2
Molecular Formula:C₂₀H₃₃N₃O₂
Molecular Weight:347.501
Hs Code.:

Synonyms:Decanedioic acid (4-amino-benzyl)-methyl-amide dimethylamide

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Chemical Property of Decanedioic acid (4-amino-benzyl)-methyl-amide dimethylamide

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Technology Process of Decanedioic acid (4-amino-benzyl)-methyl-amide dimethylamide

There total 6 articles about Decanedioic acid (4-amino-benzyl)-methyl-amide dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 74268-83-0
N,N,N'-trimethyl-N'-p-nitrobenzyl-1,10-decane diamide

: 74268-85-2
Decanedioic acid (4-amino-benzyl)-methyl-amide dimethylamide

Guidance literature:: With iron; acetic acid; In ethanol; water; for 13h; Heating;
DOI:10.1002/hlca.19800630221

Reference yield:

: 6946-46-9
9-ethoxycarbonylnonanoic acid chloride

: 74268-85-2
Decanedioic acid (4-amino-benzyl)-methyl-amide dimethylamide

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / benzene / 2 h

2: 76 percent / 1 N KOH / ethanol / Heating

3: SOCl₂ / CHCl₃ / 1.) 40 deg C, 2 h, 2.) 60 deg C, 2 h

4: benzene / 12 h

5: 95 percent / iron powder, acetic acid / ethanol; H₂O / 13 h / Heating

With potassium hydroxide; thionyl chloride; iron; acetic acid; In ethanol; chloroform; water; benzene;
DOI:10.1002/hlca.19800630221

Reference yield:

: 19499-60-6
N-methyl-4-nitrobenzylamine

: 74268-85-2
Decanedioic acid (4-amino-benzyl)-methyl-amide dimethylamide

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / benzene / 2 h

2: 76 percent / 1 N KOH / ethanol / Heating

3: SOCl₂ / CHCl₃ / 1.) 40 deg C, 2 h, 2.) 60 deg C, 2 h

4: benzene / 12 h

5: 95 percent / iron powder, acetic acid / ethanol; H₂O / 13 h / Heating

With potassium hydroxide; thionyl chloride; iron; acetic acid; In ethanol; chloroform; water; benzene;
DOI:10.1002/hlca.19800630221