3-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]propionaldehyde

Base Information

• Chemical Name: 3-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]propionaldehyde
• CAS No.: 197960-08-0
• Molecular Formula: C₁₇H₁₇ClO₆S
• Molecular Weight: 384.837
• Mol file: 197960-08-0.mol

Synonyms:3-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]propionaldehyde

Chemical Property of 3-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]propionaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]propionaldehyde

There total 1 articles about 3-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]propionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

3-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]-propanol (197960-07-9) → 3-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]propionaldehyde (197960-08-0)

Guidance literature:

With pyridine-SO₃ complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 1.38333h;

Reference yield: 72.0%

3-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]propionaldehyde (197960-08-0) + aminoguanidine nitrate (10308-82-4) → 2-[2-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]ethyl-1-methylene]hydrazinecarboximidamide nitrate (197959-50-5)

Guidance literature:

In ethanol; at 20 ℃; for 48h;

Reference yield:

3-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]propionaldehyde (197960-08-0) + 1,3-diaminoguanidine hydrochloride (36062-19-8,38360-74-6) → 2-amino-[2-[2-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]ethyl-1-methylene]hydrazine]carboximidamine (197959-19-6)

Guidance literature:

3-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]propionaldehyde; 1,3-diaminoguanidine hydrochloride; In methanol; ethanol; at 20 ℃;

With sodium hydroxide; In dichloromethane; water;

upstream raw materials:

3-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]-propanol

Downstream raw materials:

2-amino-[2-[2-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]ethyl-1-methylene]hydrazine]carboximidamine

2-[2-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]ethyl-1-methylene]hydrazinecarboximidamide nitrate

1-amino-[2-[2-[3-(5-chloro-2-methoxyphenylsulfonyloxy)-5-methylphenoxy]ethyl-1-methylene]hydrazine]carboximidamine