dichlorodicarbonyl(2-(diphenylphosphino)pyridine)ruthenium(II)

Base Information

Chemical Name:dichlorodicarbonyl(2-(diphenylphosphino)pyridine)ruthenium(II)
CAS No.:78790-90-6
Molecular Formula:C₁₉H₁₄Cl₂NO₂PRu
Molecular Weight:491.275
Hs Code.:

Synonyms:dichlorodicarbonyl(2-(diphenylphosphino)pyridine)ruthenium(II)

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Chemical Property of dichlorodicarbonyl(2-(diphenylphosphino)pyridine)ruthenium(II)

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Technology Process of dichlorodicarbonyl(2-(diphenylphosphino)pyridine)ruthenium(II)

There total 2 articles about dichlorodicarbonyl(2-(diphenylphosphino)pyridine)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 78803-80-2
3Ru*3(C₆H₅)2PC₅H₄N*9CO=(Ru((C₆H₅)2PC₅H₄N)(CO)3)3

: 78790-90-6
dichlorodicarbonyl(2-(diphenylphosphino)pyridine)ruthenium(II)

Guidance literature:: With chlorine; In dichloromethane; satd. soln. of Cl2 in CH2Cl2 added dropwise to soln. of Ru-complex in CH2Cl2, stopped after mixt. became yellow; Et2O added dropwise, filtered, washed with CH2Cl2, vac. dried;
DOI:10.1021/ic50226a005

Reference yield:

: 12107-56-1
dichloro(cycloocta-1,5-diene)palladium (II)

: 82648-71-3
bis(2-(diphenylphosphino)pyridine)tricarbonylruthenium

: 78790-90-6
RuCl2(CO)2(κ2-PPh2py)(CO)2

: 78790-91-7
[Ru(CO)2(P(C₆H₅)2(C₅H₄N))2Cl₂]

: 82648-72-4
RuPd(P(C₆H₅)2(C₅H₄N))2(CO)2Cl₂*0.5CH₂Cl₂

: 82690-70-8
RuPd(P(C₆H₅)2(C₅H₄N))2(CO)2Cl₂*1.25CH₂Cl₂

: 78055-58-0
Pd₂(2-diphenylphosphinopyridine)2Cl₂

Guidance literature:: In dichloromethane; CH2Cl2 soln. of Ru complex treated with excess of Pd complex in CH2Cl2; filtered, solvent removed in vac., fractionally crystd.;
DOI:10.1021/ic00141a020

Reference yield: 86.0%

: 37943-90-1
2-(diphenylphosphino)pyridine

: 78790-90-6
dichlorodicarbonyl(2-(diphenylphosphino)pyridine)ruthenium(II)

: 78790-91-7
dichlorodicarbonylbis(2-(diphenylphosphino)pyridine)ruthenium(II)

Guidance literature:: In dichloromethane; soln. of ligand and Ru-complex (molar ratio 2:1) in CH2Cl2 heated underreflux for 1.5 h; cooled, Et2O added dropwise, filtered, washed with Et2O, vac. dried; elem. anal.;
DOI:10.1021/ic50226a005