3,5-dithioacetic acid-3a,4a-diaza-4,4-difluoro-8-phenyl boron dipyrromethene

Base Information

• Chemical Name: 3,5-dithioacetic acid-3a,4a-diaza-4,4-difluoro-8-phenyl boron dipyrromethene
• CAS No.: 1206782-90-2
• Molecular Formula: C₁₉H₁₅BF₂N₂O₄S₂
• Molecular Weight: 448.279
• Mol file: 1206782-90-2.mol

Synonyms:3,5-dithioacetic acid-3a,4a-diaza-4,4-difluoro-8-phenyl boron dipyrromethene

Chemical Property of 3,5-dithioacetic acid-3a,4a-diaza-4,4-difluoro-8-phenyl boron dipyrromethene

Chemical Property:

Purity/Quality:

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Technology Process of 3,5-dithioacetic acid-3a,4a-diaza-4,4-difluoro-8-phenyl boron dipyrromethene

There total 1 articles about 3,5-dithioacetic acid-3a,4a-diaza-4,4-difluoro-8-phenyl boron dipyrromethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3,7-dichloro-5,5-difluoro-10-phenyl-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide + mercaptoacetic acid (68-11-1) → 3,5-dithioacetic acid-3a,4a-diaza-4,4-difluoro-8-phenyl boron dipyrromethene (1206782-90-2)

Guidance literature:

With triethylamine; In acetonitrile; for 7h; Reflux; Darkness; Inert atmosphere;

DOI:10.1016/j.bmcl.2009.10.080

Reference yield: 44.0%

3,5-dithioacetic acid-3a,4a-diaza-4,4-difluoro-8-phenyl boron dipyrromethene (1206782-90-2) + N-hydroxysulfosuccinimide sodium salt → disodium 3,5-(1-(2-(methylthio)acetoxy)-2,5-dioxopyrrolidine-3-sulfonate)-3a,4a-diaza-4,4-difluoro-8-phenyl boron dipyrromethene

Guidance literature:

With dicyclohexyl-carbodiimide; In acetonitrile; at 20 ℃;

DOI:10.1016/j.bmcl.2009.10.080

upstream raw materials:

mercaptoacetic acid