3-methyl-4,5,6,7-tetrahydro-2H-indazole

Base Information

Chemical Name:3-methyl-4,5,6,7-tetrahydro-2H-indazole
CAS No.:1967-99-3
Molecular Formula:C₈H₁₂N₂
Molecular Weight:136.197
Hs Code.:
Mol file:1967-99-3.mol

Synonyms:3-Methyl-4,5,6,7-tetrahydroindazole;NSC 220468;3-methyl-4,5,6,7-tetrahydro-2H-indazole;3-Methyl-4,5,6,7-tetrahydro-1H-indazole;

Suppliers and Price of 3-methyl-4,5,6,7-tetrahydro-2H-indazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 9 raw suppliers

Chemical Property of 3-methyl-4,5,6,7-tetrahydro-2H-indazole

Chemical Property:

Vapor Pressure:0.00203mmHg at 25°C
Refractive Index:1.564
Boiling Point:300.2 °C at 760 mmHg
Flash Point:140 °C
Density:1.097 g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-methyl-4,5,6,7-tetrahydro-2H-indazole

There total 10 articles about 3-methyl-4,5,6,7-tetrahydro-2H-indazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 874-23-7,125117-37-5
2-acetylcyclohexanone

: 1967-99-3
4,5,6,7-Tetrahydro-3-methyl-1H-indazol

Guidance literature:: With tungstate sulfuric acid; hydrazine; at 80 ℃; for 0.333333h; Green chemistry;
DOI:10.1002/jccs.201400251

Reference yield: 80.0%

: 75624-86-1
Triphenyl(4,5,6,7-tetrahydro-3-methyl-1H-indazol-7-yl)phosphonium-bromid

: 1967-99-3
4,5,6,7-Tetrahydro-3-methyl-1H-indazol

Guidance literature:: With sodium hydroxide; In water; for 1.5h; Ambient temperature;

Reference yield: 33.73%

: 932-66-1
1-cyclohexenyl methyl ketone

: 1967-99-3
4,5,6,7-Tetrahydro-3-methyl-1H-indazol

Guidance literature:: 1-cyclohexenyl methyl ketone; With hydrazine hydrate; In ethanol; at 80 ℃; for 18h;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; for 6h; Reflux;

With water; potassium hydroxide; In 1,4-dioxane; dichloromethane; for 1h;
DOI:10.1021/acsmedchemlett.7b00418