C₂₇H₃₆O₈

Base Information

Chemical Name:C₂₇H₃₆O₈
CAS No.:1449216-21-0
Molecular Formula:C₂₇H₃₆O₈
Molecular Weight:488.578
Hs Code.:

C<sub>27</sub>H<sub>36</sub>O<sub>8</sub>

Synonyms:C₂₇H₃₆O₈

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Chemical Property of C₂₇H₃₆O₈

Chemical Property:

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Technology Process of C₂₇H₃₆O₈

There total 11 articles about C₂₇H₃₆O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: C₂₇H₃₈O₈

: 1449216-21-0
C₂₇H₃₆O₈

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 0.666667h; Molecular sieve;
DOI:10.3987/COM-12-S(N)8

Reference yield:

: 1449216-13-0
C₃₆H₅₆O₄S₂Si

: 1449216-21-0
C₂₇H₃₆O₈

Guidance literature:: Multi-step reaction with 10 steps

1.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 0.5 h / 20 °C / Molecular sieve

2.1: silver(l) oxide; titanium tetrachloride; titanium(IV) isopropylate; (S)-[1,1']-binaphthalenyl-2,2'-diol / dichloromethane; diethyl ether / 21 h / -15 - 4 °C / Inert atmosphere

3.1: acetic acid / tetrahydrofuran; water / 0.83 h / 55 °C

4.1: mercury(II) perchlorate hexahydrate / dichloromethane; water; acetonitrile / 0.75 h / 4 °C

5.1: zinc(II) chloride / dichloromethane / 0.5 h / 20 °C

6.1: triethylamine; 2,4,6-trichlorobenzoyl chloride / toluene / 2 h / 20 °C

6.2: 1.5 h / 20 - 50 °C

7.1: sodium periodate; potassium permanganate / tert-butyl alcohol / 1 h / 20 °C / pH 7.2

8.1: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 11.5 h / 4 °C

9.1: triethylamine; 2,4,6-trichlorobenzoyl chloride / toluene / 3 h / 20 °C

9.2: 5 h / 4 - 20 °C

10.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 0.67 h / 20 °C / Molecular sieve

With pyridine; titanium(IV) isopropylate; potassium permanganate; sodium periodate; tetrapropylammonium perruthennate; mercury(II) perchlorate hexahydrate; 2,4,6-trichlorobenzoyl chloride; (S)-[1,1']-binaphthalenyl-2,2'-diol; titanium tetrachloride; pyridine hydrogenfluoride; acetic acid; 4-methylmorpholine N-oxide; triethylamine; zinc(II) chloride; silver(l) oxide; In tetrahydrofuran; diethyl ether; dichloromethane; water; toluene; acetonitrile; tert-butyl alcohol; 1.1: |Ley Oxidation / 9.2: |Yamaguchi Lactonization;
DOI:10.3987/COM-12-S(N)8

Reference yield:

: C₃₆H₅₄O₄S₂Si

: 1449216-21-0
C₂₇H₃₆O₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: silver(l) oxide; titanium tetrachloride; titanium(IV) isopropylate; (S)-[1,1']-binaphthalenyl-2,2'-diol / dichloromethane; diethyl ether / 21 h / -15 - 4 °C / Inert atmosphere

2.1: acetic acid / tetrahydrofuran; water / 0.83 h / 55 °C

3.1: mercury(II) perchlorate hexahydrate / dichloromethane; water; acetonitrile / 0.75 h / 4 °C

4.1: triethylamine; 2,4,6-trichlorobenzoyl chloride / toluene / 2 h / 20 °C

4.2: 1.5 h / 20 - 50 °C

5.1: sodium periodate; potassium permanganate / tert-butyl alcohol / 1 h / 20 °C / pH 7.2

6.1: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 11.5 h / 4 °C

7.1: triethylamine; 2,4,6-trichlorobenzoyl chloride / toluene / 3 h / 20 °C

7.2: 5 h / 4 - 20 °C

8.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 0.67 h / 20 °C / Molecular sieve

With pyridine; titanium(IV) isopropylate; potassium permanganate; sodium periodate; tetrapropylammonium perruthennate; mercury(II) perchlorate hexahydrate; 2,4,6-trichlorobenzoyl chloride; (S)-[1,1']-binaphthalenyl-2,2'-diol; titanium tetrachloride; pyridine hydrogenfluoride; acetic acid; 4-methylmorpholine N-oxide; triethylamine; silver(l) oxide; In tetrahydrofuran; diethyl ether; dichloromethane; water; toluene; acetonitrile; tert-butyl alcohol; 7.2: |Yamaguchi Lactonization;
DOI:10.3987/COM-12-S(N)8