(+/-)-1,3,3-trimethyl-6-[(prop-2-ynyl)oxy]-2-{[(triphenylmethyl)oxy]methyl}cyclohexene

Base Information

Chemical Name:(+/-)-1,3,3-trimethyl-6-[(prop-2-ynyl)oxy]-2-{[(triphenylmethyl)oxy]methyl}cyclohexene
CAS No.:190508-69-1
Molecular Formula:C₃₂H₃₄O₂
Molecular Weight:450.621
Hs Code.:

Synonyms:(+/-)-1,3,3-trimethyl-6-[(prop-2-ynyl)oxy]-2-{[(triphenylmethyl)oxy]methyl}cyclohexene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-1,3,3-trimethyl-6-[(prop-2-ynyl)oxy]-2-{[(triphenylmethyl)oxy]methyl}cyclohexene

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Technology Process of (+/-)-1,3,3-trimethyl-6-[(prop-2-ynyl)oxy]-2-{[(triphenylmethyl)oxy]methyl}cyclohexene

There total 4 articles about (+/-)-1,3,3-trimethyl-6-[(prop-2-ynyl)oxy]-2-{[(triphenylmethyl)oxy]methyl}cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 106-96-7
propargyl bromide

: 190508-68-0
2,4,4-Trimethyl-3-trityloxymethyl-cyclohex-2-enol

: 190508-69-1
(+/-)-1,3,3-trimethyl-6-[(prop-2-ynyl)oxy]-2-{[(triphenylmethyl)oxy]methyl}cyclohexene

Guidance literature:: With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In toluene; at 20 ℃; for 17h;

Reference yield:

: 60078-92-4,14393-38-5
2,4,4-trimethyl-3-formyl-2-cyclohexen-1-ol

: 190508-69-1
(+/-)-1,3,3-trimethyl-6-[(prop-2-ynyl)oxy]-2-{[(triphenylmethyl)oxy]methyl}cyclohexene

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / NaBH₄ / methanol / 1 h / 0 °C

2: 77 percent / triethylamine, DMAP / CH₂Cl₂ / 3 h / Heating

3: 87 percent / 60percent aq. NaOH, Bu₄NI / toluene / 17 h / 20 °C

With dmap; sodium hydroxide; sodium tetrahydroborate; tetra-(n-butyl)ammonium iodide; triethylamine; In methanol; dichloromethane; toluene;

Reference yield:

: 140887-86-1
(+/-)-3-(hydroxymethyl)-2,4,4-trimethylcyclohex-2-en-1-ol

: 190508-69-1
(+/-)-1,3,3-trimethyl-6-[(prop-2-ynyl)oxy]-2-{[(triphenylmethyl)oxy]methyl}cyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / triethylamine, DMAP / CH₂Cl₂ / 3 h / Heating

2: 87 percent / 60percent aq. NaOH, Bu₄NI / toluene / 17 h / 20 °C

With dmap; sodium hydroxide; tetra-(n-butyl)ammonium iodide; triethylamine; In dichloromethane; toluene;