N-{(R,S)-2-benzyl-3[(S)-(2-amino-4-methylthio)butyldithio]-1-oxypropyl}-L-phenylalanine benzylester

Base Information

Chemical Name:N-{(R,S)-2-benzyl-3[(S)-(2-amino-4-methylthio)butyldithio]-1-oxypropyl}-L-phenylalanine benzylester
CAS No.:141507-10-0
Molecular Formula:C₃₁H₃₈N₂O₃S₃
Molecular Weight:582.852
Hs Code.:

Synonyms:N-{(R,S)-2-benzyl-3[(S)-(2-amino-4-methylthio)butyldithio]-1-oxypropyl}-L-phenylalanine benzylester

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Chemical Property of N-{(R,S)-2-benzyl-3[(S)-(2-amino-4-methylthio)butyldithio]-1-oxypropyl}-L-phenylalanine benzylester

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Technology Process of N-{(R,S)-2-benzyl-3[(S)-(2-amino-4-methylthio)butyldithio]-1-oxypropyl}-L-phenylalanine benzylester

There total 7 articles about N-{(R,S)-2-benzyl-3[(S)-(2-amino-4-methylthio)butyldithio]-1-oxypropyl}-L-phenylalanine benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 141437-98-1
(S)-2-[(R)-2-((S)-2-tert-Butoxycarbonylamino-4-methylsulfanyl-butyldisulfanylmethyl)-3-phenyl-propionylamino]-3-phenyl-propionic acid benzyl ester

: 141507-10-0
N-{(R,S)-2-benzyl-3[(S)-(2-amino-4-methylthio)butyldithio]-1-oxypropyl}-L-phenylalanine benzylester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1021/jm00091a016

Reference yield:

: 141437-94-7
((S)-1-Mercaptomethyl-3-methylsulfanyl-propyl)-carbamic acid tert-butyl ester

: 141507-10-0
N-{(R,S)-2-benzyl-3[(S)-(2-amino-4-methylthio)butyldithio]-1-oxypropyl}-L-phenylalanine benzylester

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / CH₃COOH / ethanol / Ambient temperature

2: ethanol / Ambient temperature

3: CF₃COOH / CH₂Cl₂ / 3 h / 0 - 20 °C

With acetic acid; trifluoroacetic acid; In ethanol; dichloromethane;
DOI:10.1021/jm00091a016

Reference yield:

: 139429-04-2
Thioacetic acid S-((S)-2-tert-butoxycarbonylamino-4-methylsulfanyl-butyl) ester

: 141507-10-0
N-{(R,S)-2-benzyl-3[(S)-(2-amino-4-methylthio)butyldithio]-1-oxypropyl}-L-phenylalanine benzylester

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / 1 M NaOH / ethanol / 3 h / 0 - 20 °C

2: 75 percent / CH₃COOH / ethanol / Ambient temperature

3: ethanol / Ambient temperature

4: CF₃COOH / CH₂Cl₂ / 3 h / 0 - 20 °C

With sodium hydroxide; acetic acid; trifluoroacetic acid; In ethanol; dichloromethane;
DOI:10.1021/jm00091a016