(2R,4aR,6R,7R,8S,8aR)-7,8-bis(benzyloxy)-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-6-yl 3,4,5-tris(benzyloxy)benzoate

Base Information

Chemical Name:(2R,4aR,6R,7R,8S,8aR)-7,8-bis(benzyloxy)-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-6-yl 3,4,5-tris(benzyloxy)benzoate
CAS No.:1459719-12-0
Molecular Formula:C₅₅H₅₀O₁₀
Molecular Weight:870.996
Hs Code.:

Synonyms:(2R,4aR,6R,7R,8S,8aR)-7,8-bis(benzyloxy)-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-6-yl 3,4,5-tris(benzyloxy)benzoate

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Chemical Property of (2R,4aR,6R,7R,8S,8aR)-7,8-bis(benzyloxy)-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-6-yl 3,4,5-tris(benzyloxy)benzoate

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Technology Process of (2R,4aR,6R,7R,8S,8aR)-7,8-bis(benzyloxy)-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-6-yl 3,4,5-tris(benzyloxy)benzoate

There total 5 articles about (2R,4aR,6R,7R,8S,8aR)-7,8-bis(benzyloxy)-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-6-yl 3,4,5-tris(benzyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 1486-48-2
3,4,5-tribenzyloxybenzoic acid

: 20770-84-7,113566-69-1,113566-70-4
2,3-di-O-benzyl-4,6-O-benzylidene-D-glucopyranose

: 1459718-99-0
(2R,4aR,6S,7R,8S,8aR)-7,8-bis(benzyloxy)-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-6-yl 3,4,5-tris(benzyloxy)benzoate

: 1459719-12-0
(2R,4aR,6R,7R,8S,8aR)-7,8-bis(benzyloxy)-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-6-yl 3,4,5-tris(benzyloxy)benzoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 1459718-99-0
(2R,4aR,6S,7R,8S,8aR)-7,8-bis(benzyloxy)-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-6-yl 3,4,5-tris(benzyloxy)benzoate

: 1459719-12-0
(2R,4aR,6R,7R,8S,8aR)-7,8-bis(benzyloxy)-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-6-yl 3,4,5-tris(benzyloxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: camphor-10-sulfonic acid / acetonitrile / Reflux

2: sodium hydride

3: palladium dichloride; sodium acetate

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap

With dmap; camphor-10-sulfonic acid; sodium acetate; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium dichloride; In acetonitrile;

Reference yield:

: 48149-74-2,821794-45-0
allyl D-glucopyranoside

: 1459718-99-0
(2R,4aR,6S,7R,8S,8aR)-7,8-bis(benzyloxy)-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-6-yl 3,4,5-tris(benzyloxy)benzoate

: 1459719-12-0
(2R,4aR,6R,7R,8S,8aR)-7,8-bis(benzyloxy)-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-6-yl 3,4,5-tris(benzyloxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: camphor-10-sulfonic acid / acetonitrile / Reflux

2: sodium hydride

3: palladium dichloride; sodium acetate

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap

With dmap; camphor-10-sulfonic acid; sodium acetate; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium dichloride; In acetonitrile;