N,N'-bis<4-(2,3-dihydroxybenzamido)butyl>-2,3-dihydroxyterephthalic acid diamide

Base Information

Chemical Name:N,N'-bis<4-(2,3-dihydroxybenzamido)butyl>-2,3-dihydroxyterephthalic acid diamide
CAS No.:102212-21-5
Molecular Formula:C₃₀H₃₄N₄O₁₀
Molecular Weight:610.621
Hs Code.:

Synonyms:N,N'-bis<4-(2,3-dihydroxybenzamido)butyl>-2,3-dihydroxyterephthalic acid diamide

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Chemical Property of N,N'-bis<4-(2,3-dihydroxybenzamido)butyl>-2,3-dihydroxyterephthalic acid diamide

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Technology Process of N,N'-bis<4-(2,3-dihydroxybenzamido)butyl>-2,3-dihydroxyterephthalic acid diamide

There total 6 articles about N,N'-bis<4-(2,3-dihydroxybenzamido)butyl>-2,3-dihydroxyterephthalic acid diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: N,N'-Bis-[4-(2,3-dimethoxy-benzoylamino)-butyl]-2,3-dimethoxy-terephthalamide

: 102212-21-5
N,N'-bis<4-(2,3-dihydroxybenzamido)butyl>-2,3-dihydroxyterephthalic acid diamide

Guidance literature:: With boron tribromide; In dichloromethane; for 72h; Ambient temperature;
DOI:10.1021/jm00157a020

Reference yield:

: 1521-38-6
2,3-dimethoxybenzoic acid

: 102212-21-5
N,N'-bis<4-(2,3-dihydroxybenzamido)butyl>-2,3-dihydroxyterephthalic acid diamide

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 1 h / Heating

2: diethyl ether; dimethylsulfoxide / 1 h / Ambient temperature

3: triethylamine, 4-(dimethylamino)pyridine / dimethylformamide / 48 h / 80 °C

4: 92 percent / boron tribromide / CH₂Cl₂ / 72 h / Ambient temperature

With dmap; thionyl chloride; boron tribromide; triethylamine; In diethyl ether; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm00157a020

Reference yield:

: 7168-95-8
2,3-dimethoxyterephthalic acid

: 102212-21-5
N,N'-bis<4-(2,3-dihydroxybenzamido)butyl>-2,3-dihydroxyterephthalic acid diamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 1 h

2: triethylamine, 4-(dimethylamino)pyridine / dimethylformamide / 48 h / 80 °C

3: 92 percent / boron tribromide / CH₂Cl₂ / 72 h / Ambient temperature

With dmap; thionyl chloride; boron tribromide; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00157a020