2-{2-[4-(2-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine

Base Information

• Chemical Name: 2-{2-[4-(2-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine
• CAS No.: 89009-91-6
• Molecular Formula: C₂₅H₃₄N₄S
• Molecular Weight: 422.638

Synonyms:2-{2-[4-(2-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine

Chemical Property of 2-{2-[4-(2-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine

Chemical Property:

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Technology Process of 2-{2-[4-(2-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine

There total 1 articles about 2-{2-[4-(2-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

1-(2-methylthiophenyl)piperazine HCl (89009-93-8) + 2-(2-chloroethyl)-1,2,3,4,6,7,8,9-octahydrobenzo<1,6>naphthyridine dihydrochloride (83081-61-2) → 2-{2-[4-(2-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine (89009-91-6)

Guidance literature:

With triethylamine; In ethanol; for 2h; Heating;

DOI:10.1248/cpb.33.5332

Reference yield:

2-{2-[4-(2-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine (89009-91-6) + (2E)-but-2-enedioic acid (110-17-8,26099-09-2) → 2-<2-<4-(2-methylthiophenyl)-1-piperazinyl>ethyl>-1,2,3,4,6,7,8,9-octahydrobenzo<1,6>naphthyridine difumarate (89009-95-0)

Guidance literature:

In acetone;

DOI:10.1248/cpb.33.5332

upstream raw materials:

1-(2-methylthiophenyl)piperazine HCl

2-(2-chloroethyl)-1,2,3,4,6,7,8,9-octahydrobenzo<1,6>naphthyridine dihydrochloride

Downstream raw materials:

2-<2-<4-(2-methylthiophenyl)-1-piperazinyl>ethyl>-1,2,3,4,6,7,8,9-octahydrobenzo<1,6>naphthyridine difumarate

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