4-epi-cubebil

Base Information

• Chemical Name: 4-epi-cubebil
• CAS No.: 38230-60-3
• Molecular Formula: C₁₅H₂₆O
• Molecular Weight: 222.371

Synonyms:4-epi-cubebil

Chemical Property of 4-epi-cubebil

Chemical Property:

Purity/Quality:

99% ,98%,Electron Grade , ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 4-epi-cubebil

There total 2 articles about 4-epi-cubebil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(-)-(1R,4S,5R,6R,7S,10R)-7-isopropyl-4,10-dimethyl-tricyclo[4.4.0.01,5]decane-4-ol (23445-02-5) → 4-epi-cubebil (38230-60-3)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) NaCH₂SOMe, (ii) CS₂, (iii) MeI

2: (i) Hg(OAc)2, (ii) NaBH₄, aq. NaOH

DOI:10.1039/P19720001721

Reference yield:

α-cubebene (17699-14-8) → 4-epi-cubebil (38230-60-3)

Guidance literature:

Multistep reaction; (i) Hg(OAc)2, (ii) NaBH₄, aq. NaOH;

DOI:10.1039/P19720001721

Reference yield: 1.0%

4-epi-cubebil (38230-60-3) → cubenol (19912-67-5,21284-22-0,38757-58-3,68199-14-4,73365-77-2,81939-29-9) + 1–epi–cubenol (19912-67-5) + delta-cadinene (483-76-1,13061-82-0,16729-01-4,20085-20-5,60305-17-1,73365-79-4) + (1R,10R)-zonarene (41929-05-9)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; for 0.5h; Ambient temperature;

DOI:10.1246/bcsj.54.2366

upstream raw materials:

α-cubebene

(-)-(1R,4S,5R,6R,7S,10R)-7-isopropyl-4,10-dimethyl-tricyclo[4.4.0.0^1,5]decane-4-ol

Downstream raw materials:

cubenol

1–epi–cubenol

delta-cadinene

(1R,10R)-zonarene

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