1-(4-hydroxyphenyl)-2-ethyl-1,2-dicarba-closo-dodecaborane

Base Information

• Chemical Name: 1-(4-hydroxyphenyl)-2-ethyl-1,2-dicarba-closo-dodecaborane
• CAS No.: 1418738-53-0
• Molecular Formula: C₁₀H₂₀B₁₀O
• Molecular Weight: 264.378
• Mol file: 1418738-53-0.mol

Synonyms:1-(4-hydroxyphenyl)-2-ethyl-1,2-dicarba-closo-dodecaborane

Chemical Property of 1-(4-hydroxyphenyl)-2-ethyl-1,2-dicarba-closo-dodecaborane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(4-hydroxyphenyl)-2-ethyl-1,2-dicarba-closo-dodecaborane

There total 1 articles about 1-(4-hydroxyphenyl)-2-ethyl-1,2-dicarba-closo-dodecaborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1-(4-methoxyphenyl)-2-ethyl-1,2-dicarba-closo-dodecaborane (1427081-57-9) → 1-(4-hydroxyphenyl)-2-ethyl-1,2-dicarba-closo-dodecaborane (1418738-53-0)

Guidance literature:

With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 30h;

DOI:10.1248/cpb.c13-00796

Reference yield:

1-(4-hydroxyphenyl)-2-ethyl-1,2-dicarba-closo-dodecaborane (1418738-53-0) + C18H18BrNO4 (1418738-49-4) → C28H37B10NO5 (1427084-32-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/j.bmcl.2012.11.081

Reference yield:

1-(4-hydroxyphenyl)-2-ethyl-1,2-dicarba-closo-dodecaborane (1418738-53-0) + C21H25BBrNO4 (1418738-50-7) → C31H44B11NO5 (1427084-57-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/j.bmcl.2012.11.081

upstream raw materials:

1-(4-methoxyphenyl)-2-ethyl-1,2-dicarba-closo-dodecaborane

Downstream raw materials:

C₂₈H₃₇B₁₀NO₅

C₃₁H₄₄B₁₁NO₅