2,3-bis(p-chlorophenyl)-6,7-dihydro-5H-2a-thia-(2a-S^IV)-2,3,4a,7a-tetraazacyclopentindene-1,4(2H,3H)-dithione

Base Information

• Chemical Name: 2,3-bis(p-chlorophenyl)-6,7-dihydro-5H-2a-thia-(2a-S^IV)-2,3,4a,7a-tetraazacyclopentindene-1,4(2H,3H)-dithione
• CAS No.: 134259-08-8
• Molecular Formula: C₁₈H₁₄Cl₂N₄S₃
• Molecular Weight: 453.44

Synonyms:2,3-bis(p-chlorophenyl)-6,7-dihydro-5H-2a-thia-(2a-S^IV)-2,3,4a,7a-tetraazacyclopentindene-1,4(2H,3H)-dithione

Chemical Property of 2,3-bis(p-chlorophenyl)-6,7-dihydro-5H-2a-thia-(2a-S^IV)-2,3,4a,7a-tetraazacyclopentindene-1,4(2H,3H)-dithione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-bis(p-chlorophenyl)-6,7-dihydro-5H-2a-thia-(2a-S^IV)-2,3,4a,7a-tetraazacyclopentindene-1,4(2H,3H)-dithione

There total 1 articles about 2,3-bis(p-chlorophenyl)-6,7-dihydro-5H-2a-thia-(2a-S^IV)-2,3,4a,7a-tetraazacyclopentindene-1,4(2H,3H)-dithione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

2,3-dimethyl-6,7-dihydro-5H-2a-thia-(2a-SIV)-2,3,4a,7a-tetraazacyclopentindene-1,4(2H,3H)-dithione (72885-84-8) + 4-Chlorophenyl isothiocyanate (2131-55-7) → 6,7-dihydro-2-methyl-3-(p-chlorophenyl)-5H-1,2,4-thia(2a-SIV)-2,3,4a,7a-tetraazacyclopentindene-1,4(2H,3H)-dithione (112723-30-5) + 2,3-bis(p-chlorophenyl)-6,7-dihydro-5H-2a-thia-(2a-SIV)-2,3,4a,7a-tetraazacyclopentindene-1,4(2H,3H)-dithione (134259-08-8)

Guidance literature:

In chloroform; for 20h; Product distribution; Heating; other aryl isothiocyanates, other reaction time;

Reference yield: 99.0%

Wilkinson's catalyst (14694-95-2) + 2,3-bis(p-chlorophenyl)-6,7-dihydro-5H-2a-thia-(2a-SIV)-2,3,4a,7a-tetraazacyclopentindene-1,4(2H,3H)-dithione (134259-08-8) → Rh(P(C6H5)3)2ClNC(S)NCN(CH2)3C(S)N(ClC6H4)2

Guidance literature:

In dichloromethane; benzene; byproducts: Ph3PS; reaction at room temp. in a sealed tube (72 h);

Reference yield: 91.0%

tetrakis(triphenylphosphine) palladium(0) (14221-01-3) + 2,3-bis(p-chlorophenyl)-6,7-dihydro-5H-2a-thia-(2a-SIV)-2,3,4a,7a-tetraazacyclopentindene-1,4(2H,3H)-dithione (134259-08-8) → Pd(P(C6H5)3)NC(S)NCN(CH2)3C(S)N(ClC6H4)2

Guidance literature:

In dichloromethane; benzene; byproducts: Ph3PS; reaction at room temp. in a sealed tube (48 h);

upstream raw materials:

2,3-dimethyl-6,7-dihydro-5H-2a-thia-(2a-S^IV)-2,3,4a,7a-tetraazacyclopentindene-1,4(2H,3H)-dithione

4-Chlorophenyl isothiocyanate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 134259-08-8 2,3-bis(p-chlorophenyl)-6,7-dihydro-5H-2a-thia-(2a-S^IV)-2,3,4a,7a-tetraazacyclopentindene-1,4(2H,3H)-dithione

Send

Send

Metric Ton KG G Pound L ML

Send

Send