C₆₆H₁₂₈O₁₀Si₅

Base Information

Chemical Name:C₆₆H₁₂₈O₁₀Si₅
CAS No.:902132-50-7
Molecular Formula:C₆₆H₁₂₈O₁₀Si₅
Molecular Weight:1222.16
Hs Code.:

C<sub>66</sub>H<sub>128</sub>O<sub>10</sub>Si<sub>5</sub>

Synonyms:C₆₆H₁₂₈O₁₀Si₅

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Chemical Property of C₆₆H₁₂₈O₁₀Si₅

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Technology Process of C₆₆H₁₂₈O₁₀Si₅

There total 34 articles about C₆₆H₁₂₈O₁₀Si₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 902132-48-3
C₇₁H₁₃₆O₁₁Si₅

: 902132-50-7
C₆₆H₁₂₈O₁₀Si₅

Guidance literature:: With lithium triethylborohydride; In tetrahydrofuran; at 0 ℃; for 1.5h;
DOI:10.1039/b602020h

Reference yield:

: 902132-11-0
(3R,4S)-3-(4-methoxybenzyloxy)-4-methyl-5-hexenal

: 902132-50-7
C₆₆H₁₂₈O₁₀Si₅

Guidance literature:: Multi-step reaction with 14 steps

1.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -78 °C

1.2: tetrahydrofuran; hexane / 2 h / -78 - 0 °C

2.1: 93 percent / imidazole; 4-DMAP / CH₂Cl₂ / 2 h / 20 °C

3.1: O₃ / CH₂Cl₂ / -78 °C

3.2: 98 percent / PPh₃ / CH₂Cl₂ / 1 h / -78 - 25 °C

4.1: 98 percent / benzene / 16 h / 70 °C

5.1: 99 percent / DIBAL-H / tetrahydrofuran / 0.5 h / 0 °C

6.1: Et₃N / tetrahydrofuran / 1 h / 0 °C

7.1: 2.004 g / LiBr / tetrahydrofuran / 0.75 h / 25 °C

8.1: LDA / tetrahydrofuran / 1.5 h / -78 °C

8.2: 84 percent / tetrahydrofuran / 1 h / -78 °C

9.1: LDA / tetrahydrofuran / 2 h / -78 °C

9.2: tetrahydrofuran / 4 h / -78 °C

10.1: 1.811 g / aq. (CO₂H)2 / diethyl ether / 40 h / 25 °C

11.1: 64 percent / TsOH*H₂O / methanol; CH₂Cl₂ / 20 h / 25 °C

12.1: 54 percent / 2,6-lutidine / CH₂Cl₂ / 1.5 h / 0 °C

13.1: 84 percent / K₂CO₃ / methanol; diethyl ether / 4 h / 25 °C

14.1: 74 percent / Super Hydride(R) / tetrahydrofuran / 1.5 h / 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; dmap; n-butyllithium; oxalic acid; diisobutylaluminium hydride; lithium triethylborohydride; potassium carbonate; toluene-4-sulfonic acid; ozone; triethylamine; lithium bromide; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; benzene; 4.1: Wittig reaction;
DOI:10.1039/b602020h

Reference yield:

: 902131-93-5
C₃₉H₇₇IO₅Si₃

: 902132-50-7
C₆₆H₁₂₈O₁₀Si₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: 90 percent / DDQ; aq. pH 7.0 buffer / CH₂Cl₂ / 1 h / 25 °C

2.1: 65 percent / pyridine; 4-DMAP / CH₂Cl₂ / 22 h / 0 - 25 °C

3.1: LDA / tetrahydrofuran / 2 h / -78 °C

3.2: tetrahydrofuran / 4 h / -78 °C

4.1: 1.811 g / aq. (CO₂H)2 / diethyl ether / 40 h / 25 °C

5.1: 64 percent / TsOH*H₂O / methanol; CH₂Cl₂ / 20 h / 25 °C

6.1: 54 percent / 2,6-lutidine / CH₂Cl₂ / 1.5 h / 0 °C

7.1: 84 percent / K₂CO₃ / methanol; diethyl ether / 4 h / 25 °C

8.1: 74 percent / Super Hydride(R) / tetrahydrofuran / 1.5 h / 0 °C

With pyridine; 2,6-dimethylpyridine; dmap; oxalic acid; lithium triethylborohydride; potassium carbonate; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1039/b602020h