Phthalic acid 1-[(2S,3R,4S,5S,6R)-6-(tert-butyl-diphenyl-silanyloxymethyl)-4,5-dihydroxy-2-methoxy-tetrahydro-pyran-3-yl] ester 2-((2R,3R,4S,5R,6S)-3,4,5-triacetoxy-6-phenylsulfanyl-tetrahydro-pyran-2-ylmethyl) ester

Base Information

Chemical Name:Phthalic acid 1-[(2S,3R,4S,5S,6R)-6-(tert-butyl-diphenyl-silanyloxymethyl)-4,5-dihydroxy-2-methoxy-tetrahydro-pyran-3-yl] ester 2-((2R,3R,4S,5R,6S)-3,4,5-triacetoxy-6-phenylsulfanyl-tetrahydro-pyran-2-ylmethyl) ester
CAS No.:172223-32-4
Molecular Formula:C₄₉H₅₆O₁₆SSi
Molecular Weight:961.126
Hs Code.:

Phthalic acid 1-[(2S,3R,4S,5S,6R)-6-(tert-butyl-diphenyl-silanyloxymethyl)-4,5-dihydroxy-2-methoxy-tetrahydro-pyran-3-yl] ester 2-((2R,3R,4S,5R,6S)-3,4,5-triacetoxy-6-phenylsulfanyl-tetrahydro-pyran-2-ylmethyl) ester

Synonyms:Phthalic acid 1-[(2S,3R,4S,5S,6R)-6-(tert-butyl-diphenyl-silanyloxymethyl)-4,5-dihydroxy-2-methoxy-tetrahydro-pyran-3-yl] ester 2-((2R,3R,4S,5R,6S)-3,4,5-triacetoxy-6-phenylsulfanyl-tetrahydro-pyran-2-ylmethyl) ester

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Chemical Property of Phthalic acid 1-[(2S,3R,4S,5S,6R)-6-(tert-butyl-diphenyl-silanyloxymethyl)-4,5-dihydroxy-2-methoxy-tetrahydro-pyran-3-yl] ester 2-((2R,3R,4S,5R,6S)-3,4,5-triacetoxy-6-phenylsulfanyl-tetrahydro-pyran-2-ylmethyl) ester

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Technology Process of Phthalic acid 1-[(2S,3R,4S,5S,6R)-6-(tert-butyl-diphenyl-silanyloxymethyl)-4,5-dihydroxy-2-methoxy-tetrahydro-pyran-3-yl] ester 2-((2R,3R,4S,5R,6S)-3,4,5-triacetoxy-6-phenylsulfanyl-tetrahydro-pyran-2-ylmethyl) ester

There total 1 articles about Phthalic acid 1-[(2S,3R,4S,5S,6R)-6-(tert-butyl-diphenyl-silanyloxymethyl)-4,5-dihydroxy-2-methoxy-tetrahydro-pyran-3-yl] ester 2-((2R,3R,4S,5R,6S)-3,4,5-triacetoxy-6-phenylsulfanyl-tetrahydro-pyran-2-ylmethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58479-62-2
(2R,3S,4S,5R,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methoxy-tetrahydro-pyran-3,4,5-triol

: 2-Chlorocarbonyl-benzoic acid (2R,3R,4S,5R,6S)-3,4,5-triacetoxy-6-phenylsulfanyl-tetrahydro-pyran-2-ylmethyl ester

: 172223-32-4
Phthalic acid 1-[(2S,3R,4S,5S,6R)-6-(tert-butyl-diphenyl-silanyloxymethyl)-4,5-dihydroxy-2-methoxy-tetrahydro-pyran-3-yl] ester 2-((2R,3R,4S,5R,6S)-3,4,5-triacetoxy-6-phenylsulfanyl-tetrahydro-pyran-2-ylmethyl) ester

Guidance literature:: With di(n-butyl)tin oxide; Irradiation; microwave;
DOI:10.1039/c39950002005

Reference yield: 80.0%

: 172223-32-4
Phthalic acid 1-[(2S,3R,4S,5S,6R)-6-(tert-butyl-diphenyl-silanyloxymethyl)-4,5-dihydroxy-2-methoxy-tetrahydro-pyran-3-yl] ester 2-((2R,3R,4S,5R,6S)-3,4,5-triacetoxy-6-phenylsulfanyl-tetrahydro-pyran-2-ylmethyl) ester

: C₄₃H₅₀O₁₆Si

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane; Ambient temperature;
DOI:10.1039/c39950002005

Reference yield:

: 172223-32-4
Phthalic acid 1-[(2S,3R,4S,5S,6R)-6-(tert-butyl-diphenyl-silanyloxymethyl)-4,5-dihydroxy-2-methoxy-tetrahydro-pyran-3-yl] ester 2-((2R,3R,4S,5R,6S)-3,4,5-triacetoxy-6-phenylsulfanyl-tetrahydro-pyran-2-ylmethyl) ester

: C₄₃H₅₀O₁₆Si

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane; at -78 ℃;
DOI:10.1016/0040-4039(95)02316-X