[((C₆H₄CH₂N(CH₃)2)Pd)2Cl(P(C₆H₅)2CH(CN))]

Base Information

Chemical Name:[((C₆H₄CH₂N(CH₃)2)Pd)2Cl(P(C₆H₅)2CH(CN))]
CAS No.:79079-79-1
Molecular Formula:C₃₂H₃₅ClN₃PPd₂
Molecular Weight:740.917
Hs Code.:

[((C<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>N(CH<sub>3</sub>)2)Pd)2Cl(P(C<sub>6</sub>H<sub>5</sub>)2CH(CN))]

Synonyms:[((C₆H₄CH₂N(CH₃)2)Pd)2Cl(P(C₆H₅)2CH(CN))]

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Chemical Property of [((C₆H₄CH₂N(CH₃)2)Pd)2Cl(P(C₆H₅)2CH(CN))]

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Technology Process of [((C₆H₄CH₂N(CH₃)2)Pd)2Cl(P(C₆H₅)2CH(CN))]

There total 2 articles about [((C₆H₄CH₂N(CH₃)2)Pd)2Cl(P(C₆H₅)2CH(CN))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: bis[(benzyldimethylamino)chloropalladium(II)]

: 31201-88-4
diphenylphosphanyl-acetonitrile

: 79079-79-1
[((C₆H₄CH₂N(CH₃)2)Pd)2Cl(P(C₆H₅)2CH(CN))]

Guidance literature:: With N-isopropylcyclohexylamine; n-C₄H₉Li; In tetrahydrofuran; under Ar to N-isopropylcyclohexylamine in THF added at -20°C 1.73 M hexane soln. of n-BuLi, after 0.5 h, this soln. added at -5°Cto Ph2PCH2CN in THF, this added to Pd-compd. in THF at -10°C, mixt. stirred for 0.5 h; pentane added, after 3 h at room temp. crystals collected, recrystd. from THF/pentane; elem. anal.;
DOI:10.1021/ja00407a028

Reference yield:

: bis[(benzyldimethylamino)chloropalladium(II)]

: 86632-52-2
LiCH(CN)(P(C₆H₅)2)

: 79079-79-1
[((C₆H₄CH₂N(CH₃)2)Pd)2Cl(P(C₆H₅)2CH(CN))]

: 86632-51-1
[((C₆H₄CH₂N(CH₃)2)Pd)2Cl(P(C₆H₅)2CH₂C(NH)C(CN)P(C₆H₅)2)]

Guidance literature:: In tetrahydrofuran; to stirred suspn. of Pd complex in THF added soln. of Li(CH(CN)PPh2) (2equiv) in THF at -10 °C under Ar, stirred for 0.5 h; added pentane, ppt. of ((C6H4CH2NMe2)2Pd2Cl(PPh2CH(CN)) sepd., pptd. ((C6H4CH2NMe2)2Pd2Cl(Ph2PCH2C(NH)C(CN)PPh2)) by addn. of pentane to motherliquor;