C₁₇H₁₁BrNOP

Base Information

Chemical Name:C₁₇H₁₁BrNOP
CAS No.:1312012-50-2
Molecular Formula:C₁₇H₁₁BrNOP
Molecular Weight:356.158
Hs Code.:

Synonyms:C₁₇H₁₁BrNOP

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Chemical Property of C₁₇H₁₁BrNOP

Chemical Property:

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Technology Process of C₁₇H₁₁BrNOP

There total 6 articles about C₁₇H₁₁BrNOP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1312012-57-9
C₁₁H₇NP(O)C₆H₅

: 1312012-50-2
C₁₇H₁₁BrNOP

Guidance literature:: With N-Bromosuccinimide; sulfuric acid; trifluoroacetic acid; at 0 ℃; Inert atmosphere; Darkness;
DOI:10.1021/ic200951x

Reference yield:

: 244205-40-1
(2-bromophenyl)boronic acid

: 1312012-50-2
C₁₇H₁₁BrNOP

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tetrahydrofuran; water / 72 h / Inert atmosphere; Reflux

2.1: phosphorus tribromide / 40 h / 140 °C / Inert atmosphere

3.1: tert.-butyl lithium / diethyl ether; pentane / 1 h / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: dihydrogen peroxide / chloroform; water / 2 h / Inert atmosphere

5.1: N-Bromosuccinimide; sulfuric acid; trifluoroacetic acid / 0 °C / Inert atmosphere; Darkness

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; dihydrogen peroxide; tert.-butyl lithium; phosphorus tribromide; potassium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; chloroform; water; pentane; 1.1: Suzuki-Miyaura coupling;
DOI:10.1021/ic200951x

Reference yield:

: 78607-36-0
2-chloro-3-iodopyridine

: 1312012-50-2
C₁₇H₁₁BrNOP

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tetrahydrofuran; water / 72 h / Inert atmosphere; Reflux

2.1: phosphorus tribromide / 40 h / 140 °C / Inert atmosphere

3.1: tert.-butyl lithium / diethyl ether; pentane / 1 h / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: dihydrogen peroxide / chloroform; water / 2 h / Inert atmosphere

5.1: N-Bromosuccinimide; sulfuric acid; trifluoroacetic acid / 0 °C / Inert atmosphere; Darkness

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; dihydrogen peroxide; tert.-butyl lithium; phosphorus tribromide; potassium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; chloroform; water; pentane; 1.1: Suzuki-Miyaura coupling;
DOI:10.1021/ic200951x