((2R,5R)-4-(4-methoxybenzyloxy)-2-methyltetrahydrofuran-2,5-diyl)dimethanol

Base Information

Chemical Name:((2R,5R)-4-(4-methoxybenzyloxy)-2-methyltetrahydrofuran-2,5-diyl)dimethanol
CAS No.:1313493-14-9
Molecular Formula:C₁₅H₂₂O₅
Molecular Weight:282.337
Hs Code.:

Synonyms:((2R,5R)-4-(4-methoxybenzyloxy)-2-methyltetrahydrofuran-2,5-diyl)dimethanol

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Chemical Property of ((2R,5R)-4-(4-methoxybenzyloxy)-2-methyltetrahydrofuran-2,5-diyl)dimethanol

Chemical Property:

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Technology Process of ((2R,5R)-4-(4-methoxybenzyloxy)-2-methyltetrahydrofuran-2,5-diyl)dimethanol

There total 3 articles about ((2R,5R)-4-(4-methoxybenzyloxy)-2-methyltetrahydrofuran-2,5-diyl)dimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1313493-11-6
(2R)-3-(4-methoxybenzyloxy)-5-methylhex-5-ene-1,2-diol

: 1313493-14-9
((2R,5R)-4-(4-methoxybenzyloxy)-2-methyltetrahydrofuran-2,5-diyl)dimethanol

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1021/jo200899v

Reference yield:

: 1-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-3-methyl-but-3-en-1-ol

: 1313493-14-9
((2R,5R)-4-(4-methoxybenzyloxy)-2-methyltetrahydrofuran-2,5-diyl)dimethanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C

1.2: 2 h / 0 - 20 °C

2.1: water; acetic acid / tetrahydrofuran / 15 h / 40 °C

3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 16 h / 20 °C

With tetrapropylammonium perruthennate; water; sodium hydride; acetic acid; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo200899v

Reference yield:

: 1313493-13-8
(4R)-4-(1-(4-methoxybenzyloxy)-3-methylbut-3-en-1-yl)-2,2-dimethyl-1,3-dioxolane

: 1313493-14-9
((2R,5R)-4-(4-methoxybenzyloxy)-2-methyltetrahydrofuran-2,5-diyl)dimethanol

Guidance literature:: Multi-step reaction with 2 steps

1: water; acetic acid / tetrahydrofuran / 15 h / 40 °C

2: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 16 h / 20 °C

With tetrapropylammonium perruthennate; water; acetic acid; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo200899v