thioacetic acid S-{1-[2-(2-acetylsulfanyl-2-methylpropionylamino)phenylcarbamoyl]-1-methylethyl} ester

Base Information

• Chemical Name: thioacetic acid S-{1-[2-(2-acetylsulfanyl-2-methylpropionylamino)phenylcarbamoyl]-1-methylethyl} ester
• CAS No.: 186357-20-0
• Molecular Formula: C₁₈H₂₄N₂O₄S₂
• Molecular Weight: 396.532

Synonyms:thioacetic acid S-{1-[2-(2-acetylsulfanyl-2-methylpropionylamino)phenylcarbamoyl]-1-methylethyl} ester

Chemical Property of thioacetic acid S-{1-[2-(2-acetylsulfanyl-2-methylpropionylamino)phenylcarbamoyl]-1-methylethyl} ester

Chemical Property:

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Technology Process of thioacetic acid S-{1-[2-(2-acetylsulfanyl-2-methylpropionylamino)phenylcarbamoyl]-1-methylethyl} ester

There total 2 articles about thioacetic acid S-{1-[2-(2-acetylsulfanyl-2-methylpropionylamino)phenylcarbamoyl]-1-methylethyl} ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-diamino-benzene (95-54-5) → thioacetic acid S-{1-[2-(2-acetylsulfanyl-2-methylpropionylamino)phenylcarbamoyl]-1-methylethyl} ester (186357-20-0)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N

With triethylamine;

Reference yield:

1,2-bis(2-bromo-2-methylpropanamido)benzene (136667-95-3) → thioacetic acid S-{1-[2-(2-acetylsulfanyl-2-methylpropionylamino)phenylcarbamoyl]-1-methylethyl} ester (186357-20-0)

Guidance literature:

Reference yield: 95.0%

thioacetic acid S-{1-[2-(2-acetylsulfanyl-2-methylpropionylamino)phenylcarbamoyl]-1-methylethyl} ester (186357-20-0) → 2-mercapto-N-[2-(2-mercapto-2-methylpropionylamino)phenyl]-2-methylpropionamide (469867-87-6)

Guidance literature:

With potassium carbonate; In methanol;

DOI:10.1016/j.tet.2007.01.002

upstream raw materials:

1,2-bis(2-bromo-2-methylpropanamido)benzene

1,2-diamino-benzene

Downstream raw materials:

2-mercapto-N-[2-(2-mercapto-2-methylpropionylamino)phenyl]-2-methylpropionamide

K⁽¹⁺⁾*P(C₆H₅)4⁽¹⁺⁾*Ni(C₆H₄(NCOC(CH₃)2S)2)^(2-) = K[P(C₆H₅)4][Ni(C₆H₄(NCOC(CH₃)2S)2)]

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