C₂₃H₂₂N₂O

Base Information

Chemical Name:C₂₃H₂₂N₂O
CAS No.:1188489-56-6
Molecular Formula:C₂₃H₂₂N₂O
Molecular Weight:342.44
Hs Code.:

C<sub>23</sub>H<sub>22</sub>N<sub>2</sub>O

Synonyms:C₂₃H₂₂N₂O

Suppliers and Price of C₂₃H₂₂N₂O

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₃H₂₂N₂O

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₃H₂₂N₂O

There total 12 articles about C₂₃H₂₂N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1188489-29-3
C₂₄H₂₄N₂O

: 1188489-56-6
C₂₃H₂₂N₂O

Guidance literature:: With hydrogenchloride; water; In 1,4-dioxane; at 80 ℃; for 5h;

Reference yield:

: 670-80-4
4-cyclohexen-1-ylmorpholine

: 1188489-56-6
C₂₃H₂₂N₂O

Guidance literature:: Multi-step reaction with 10 steps

1.1: dichloromethane / 20 °C

2.1: sulfuric acid / 0.5 h / 100 °C

3.1: sulfuric acid / 0.25 h / 100 °C

4.1: trichlorophosphate / Reflux

5.1: methanol / 20 °C / Reflux

6.1: bis-triphenylphosphine-palladium(II) chloride / toluene / 18 h / 80 °C / Inert atmosphere

7.1: potassium tert-butylate / methanol; dimethyl sulfoxide / 10 °C / Inert atmosphere

7.2: 1.25 h / 10 °C

8.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 °C / Inert atmosphere

8.2: 18 h / 20 °C

8.3: 3 h

9.1: Chiralpak_.(R). / ethanol; carbon dioxide; isopropylamine; isopropyl alcohol / Resolution of racemate

10.1: hydrogenchloride; water / 1,4-dioxane / 5 h / 80 °C

With hydrogenchloride; sulfuric acid; potassium tert-butylate; water; sodium hydride; trichlorophosphate; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; methanol; ethanol; dichloromethane; carbon dioxide; dimethyl sulfoxide; isopropylamine; N,N-dimethyl-formamide; isopropyl alcohol; toluene; mineral oil;

Reference yield:

: 1188489-22-6
C₁₃H₁₄BrNO₂

: 1188489-56-6
C₂₃H₂₂N₂O

Guidance literature:: Multi-step reaction with 8 steps

1.1: sulfuric acid / 0.25 h / 100 °C

2.1: trichlorophosphate / Reflux

3.1: methanol / 20 °C / Reflux

4.1: bis-triphenylphosphine-palladium(II) chloride / toluene / 18 h / 80 °C / Inert atmosphere

5.1: potassium tert-butylate / methanol; dimethyl sulfoxide / 10 °C / Inert atmosphere

5.2: 1.25 h / 10 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 °C / Inert atmosphere

6.2: 18 h / 20 °C

6.3: 3 h

7.1: Chiralpak_.(R). / ethanol; carbon dioxide; isopropylamine; isopropyl alcohol / Resolution of racemate

8.1: hydrogenchloride; water / 1,4-dioxane / 5 h / 80 °C

With hydrogenchloride; sulfuric acid; potassium tert-butylate; water; sodium hydride; trichlorophosphate; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; methanol; ethanol; carbon dioxide; dimethyl sulfoxide; isopropylamine; N,N-dimethyl-formamide; isopropyl alcohol; toluene; mineral oil;