1,2-dideoxy-1β-[4-(2-naphthyl)phenyl]-3,5-di-O-(4-toluoyl)-D-ribofuranose

Base Information

Chemical Name:1,2-dideoxy-1β-[4-(2-naphthyl)phenyl]-3,5-di-O-(4-toluoyl)-D-ribofuranose
CAS No.:872051-22-4
Molecular Formula:C₃₇H₃₂O₅
Molecular Weight:556.658
Hs Code.:

Synonyms:1,2-dideoxy-1β-[4-(2-naphthyl)phenyl]-3,5-di-O-(4-toluoyl)-D-ribofuranose

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Chemical Property of 1,2-dideoxy-1β-[4-(2-naphthyl)phenyl]-3,5-di-O-(4-toluoyl)-D-ribofuranose

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Technology Process of 1,2-dideoxy-1β-[4-(2-naphthyl)phenyl]-3,5-di-O-(4-toluoyl)-D-ribofuranose

There total 4 articles about 1,2-dideoxy-1β-[4-(2-naphthyl)phenyl]-3,5-di-O-(4-toluoyl)-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 872051-17-7
1-β-(4-bromophenyl)-1,2-dideoxy-3,5-di-O-(4-toluoyl)-D-ribofuranose

: 32316-92-0
naphthalene-2-boronic acid

: 872051-22-4
1,2-dideoxy-1β-[4-(2-naphthyl)phenyl]-3,5-di-O-(4-toluoyl)-D-ribofuranose

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In toluene; at 100 ℃; for 12h;
DOI:10.1002/ejoc.200500607

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 872051-22-4
1,2-dideoxy-1β-[4-(2-naphthyl)phenyl]-3,5-di-O-(4-toluoyl)-D-ribofuranose

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium; ethylene bromide / tetrahydrofuran / 1 h / 65 °C

1.2: 12 percent / tetrahydrofuran / 12 h / 20 °C

2.1: 71 percent / K₂CO₃; Pd(PPh₃)4 / toluene / 12 h / 100 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; magnesium; ethylene dibromide; In tetrahydrofuran; toluene; 2.1: Suzuki-Miyaura cross-coupling reaction;
DOI:10.1002/ejoc.200500607

Reference yield:

: 4330-21-6
2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride

: 872051-22-4
1,2-dideoxy-1β-[4-(2-naphthyl)phenyl]-3,5-di-O-(4-toluoyl)-D-ribofuranose

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium; ethylene bromide / tetrahydrofuran / 1 h / 65 °C

1.2: 12 percent / tetrahydrofuran / 12 h / 20 °C

2.1: 71 percent / K₂CO₃; Pd(PPh₃)4 / toluene / 12 h / 100 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; magnesium; ethylene dibromide; In tetrahydrofuran; toluene; 2.1: Suzuki-Miyaura cross-coupling reaction;
DOI:10.1002/ejoc.200500607