benzyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-O-(3-O-benzyl-α-D-xylopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:benzyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-O-(3-O-benzyl-α-D-xylopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:132628-08-1
Molecular Formula:C₈₀H₈₄O₁₅
Molecular Weight:1285.54
Hs Code.:

Synonyms:benzyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-O-(3-O-benzyl-α-D-xylopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of benzyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-O-(3-O-benzyl-α-D-xylopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of benzyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-O-(3-O-benzyl-α-D-xylopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 11 articles about benzyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-O-(3-O-benzyl-α-D-xylopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 132628-07-0
benzyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-O-(2,3-anhydro-α-D-ribopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 100-51-6,185532-71-2
benzyl alcohol

: 132628-08-1
benzyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-O-(3-O-benzyl-α-D-xylopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With sodium hydride; at 100 ℃; for 5h;
DOI:10.1016/0008-6215(91)80154-F

Reference yield:

: 25320-59-6
tetra-O-benzyl glucopyranosyl chloride

: 132628-08-1
benzyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-O-(3-O-benzyl-α-D-xylopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / AgClO₄, 2,4,6-trimethylpyridine / 1,2-dimethoxy-ethane; diethyl ether / Ambient temperature

2: 76 percent / sodium hydride / 5 h / 100 °C

With 2,4,6-trimethyl-pyridine; silver perchlorate; sodium hydride; In 1,2-dimethoxyethane; diethyl ether;
DOI:10.1016/0008-6215(91)80154-F

Reference yield:

: 67831-42-9
benzyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 132628-08-1
benzyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->4)-O-(3-O-benzyl-α-D-xylopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 8 steps

1: 80 percent / dimethyl(methylthio)sulfonium triflate (DMTST) / CH₂Cl₂ / 2 h / Ambient temperature

2: 92 percent / methanolic M NaOMe / CH₂Cl₂ / 2 h / Ambient temperature

3: 86 percent / p-toluenesulfonic acid / dimethylformamide / 3 h / Ambient temperature

4: 84 percent / pyridine / 3 h / Ambient temperature

5: 90 percent / water / acetic acid / 0.33 h / 90 °C

6: 83 percent / Na / methanol / Ambient temperature

7: 67 percent / AgClO₄, 2,4,6-trimethylpyridine / 1,2-dimethoxy-ethane; diethyl ether / Ambient temperature

8: 76 percent / sodium hydride / 5 h / 100 °C

With 2,4,6-trimethyl-pyridine; water; sodium methylate; silver perchlorate; sodium; sodium hydride; toluene-4-sulfonic acid; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In pyridine; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(91)80154-F