1-[6-(2-(2-methyl-4-bromobenzyloxy)-phenyl)pyridin-2-yl]-2-methyl-pyrrole-3-carboxylic acid

Base Information

Chemical Name:1-[6-(2-(2-methyl-4-bromobenzyloxy)-phenyl)pyridin-2-yl]-2-methyl-pyrrole-3-carboxylic acid
CAS No.:1160433-99-7
Molecular Formula:C₂₅H₂₁BrN₂O₃
Molecular Weight:477.357
Hs Code.:

Synonyms:1-[6-(2-(2-methyl-4-bromobenzyloxy)-phenyl)pyridin-2-yl]-2-methyl-pyrrole-3-carboxylic acid

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Chemical Property of 1-[6-(2-(2-methyl-4-bromobenzyloxy)-phenyl)pyridin-2-yl]-2-methyl-pyrrole-3-carboxylic acid

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Technology Process of 1-[6-(2-(2-methyl-4-bromobenzyloxy)-phenyl)pyridin-2-yl]-2-methyl-pyrrole-3-carboxylic acid

There total 1 articles about 1-[6-(2-(2-methyl-4-bromobenzyloxy)-phenyl)pyridin-2-yl]-2-methyl-pyrrole-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1160431-28-6
C₁₉H₁₈N₂O₃

: 156001-49-9
4-bromo-2-methylbenzyl bromide

: 1160433-99-7
1-[6-(2-(2-methyl-4-bromobenzyloxy)-phenyl)pyridin-2-yl]-2-methyl-pyrrole-3-carboxylic acid

Guidance literature:: C₁₉H₁₈N₂O₃; 4-bromo-2-methylbenzyl bromide; With caesium carbonate; In acetonitrile; for 10h; Heating / reflux;

With sodium hydroxide; ethanol; water; In tetrahydrofuran; at 70 ℃; for 48h;

With hydrogenchloride; water; In tetrahydrofuran; ethanol; pH=5;

Reference yield: 15.46%

: 1160433-99-7
1-[6-(2-(2-methyl-4-bromobenzyloxy)-phenyl)pyridin-2-yl]-2-methyl-pyrrole-3-carboxylic acid

: 1765-93-1
4-fluoroboronic acid

: 1160430-27-2
1-[6-(2-(2-methyl-4-(4-fluorophenyl)benzyloxy)-phenyl)pyridin-2-yl]-2-methyl-pyrrole-3-carboxylic acid

Guidance literature:: 1-[6-(2-(2-methyl-4-bromobenzyloxy)-phenyl)pyridin-2-yl]-2-methyl-pyrrole-3-carboxylic acid; 4-fluoroboronic acid; With caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; ethanol; at 130 ℃; for 0.133333h; Microwave irradiation;

With hydrogenchloride; water; In ethanol; 1,2-dichloro-ethane; pH=5;