3,3'-(4,4'-(9H-fluorene-9,9-diyl)bis(4,1-phenylene))bis(oxy)dipopane-1,2-diol

Base Information

Chemical Name:3,3'-(4,4'-(9H-fluorene-9,9-diyl)bis(4,1-phenylene))bis(oxy)dipopane-1,2-diol
CAS No.:507219-58-1
Molecular Formula:C₃₁H₃₀O₆
Molecular Weight:498.576
Hs Code.:

Synonyms:3,3'-(4,4'-(9H-fluorene-9,9-diyl)bis(4,1-phenylene))bis(oxy)dipopane-1,2-diol

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Chemical Property of 3,3'-(4,4'-(9H-fluorene-9,9-diyl)bis(4,1-phenylene))bis(oxy)dipopane-1,2-diol

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Technology Process of 3,3'-(4,4'-(9H-fluorene-9,9-diyl)bis(4,1-phenylene))bis(oxy)dipopane-1,2-diol

There total 4 articles about 3,3'-(4,4'-(9H-fluorene-9,9-diyl)bis(4,1-phenylene))bis(oxy)dipopane-1,2-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 9,9-bis[4-(2,3-epoxypropoxy)phenyl]fluorene

: 507219-58-1
3,3'-(4,4'-(9H-fluorene-9,9-diyl)bis(4,1-phenylene))bis(oxy)dipopane-1,2-diol

Guidance literature:: With water; bismuth(lll) trifluoromethanesulfonate; In propargyl alcohol; acetonitrile; at 20 ℃; for 44h;

Reference yield: 17.0%

: 9,9-bis[4-(2,3-epoxypropoxy)phenyl]fluorene

: 107-19-7
propargyl alcohol

: 507219-58-1
3,3'-(4,4'-(9H-fluorene-9,9-diyl)bis(4,1-phenylene))bis(oxy)dipopane-1,2-diol

: 1403963-48-3
3-(4-(9-(4-(2-hydroxy-3-(prop-2-ynyloxy)propoxy)phenyl)-9H-fluoren-9-yl)phenoxy)propane-1,2-diol

Guidance literature:: With water; bismuth(lll) trifluoromethanesulfonate; In acetonitrile; at 20 ℃; for 44h;

Reference yield:

: 3236-71-3
9,9-bis(4-hydroxyphenyl)fluorene

: 507219-58-1
3,3'-(4,4'-(9H-fluorene-9,9-diyl)bis(4,1-phenylene))bis(oxy)dipopane-1,2-diol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C / Inert atmosphere

1.2: 162 h / 20 °C

2.1: water / bismuth(lll) trifluoromethanesulfonate / acetonitrile; propargyl alcohol / 44 h / 20 °C

With water; sodium hydride; bismuth(lll) trifluoromethanesulfonate; In propargyl alcohol; N,N-dimethyl-formamide; acetonitrile; mineral oil;